as-made PST-33 Goniometer: PW3050/60 (Theta/Theta) Cu K(alpha)1,2 ----- 5.006565140 1604.0 5.019695423 1558.0 5.032825705 1565.0 5.045955988 1716.0 5.059086271 1540.0 5.072216553 1597.0 5.085346836 1547.0 5.098477119 1574.0 5.111607401 1623.0 5.124737684 1718.0 5.137867967 1632.0 5.150998249 1600.0 5.164128532 1579.0 5.177258815 1646.0 5.190389097 1606.0 5.203519380 1759.0 5.216649663 1598.0 5.229779946 1552.0 5.242910228 1603.0 5.256040511 1635.0 5.269170794 1555.0 5.282301076 1589.0 5.295431359 1571.0 5.308561642 1633.0 5.321691924 1604.0 5.334822207 1698.0 5.347952490 1603.0 5.361082772 1580.0 5.374213055 1646.0 5.387343338 1540.0 5.400473620 1641.0 5.413603903 1634.0 5.426734186 1623.0 5.439864468 1582.0 5.452994751 1622.0 5.466125034 1678.0 5.479255316 1603.0 5.492385599 1549.0 5.505515882 1567.0 5.518646164 1680.0 5.531776447 1599.0 5.544906730 1602.0 5.558037012 1705.0 5.571167295 1604.0 5.584297578 1579.0 5.597427860 1586.0 5.610558143 1563.0 5.623688426 1612.0 5.636818708 1582.0 5.649948991 1746.0 5.663079274 1710.0 5.676209557 1599.0 5.689339839 1626.0 5.702470122 1680.0 5.715600405 1505.0 5.728730687 1520.0 5.741860970 1583.0 5.754991253 1667.0 5.768121535 1632.0 5.781251818 1553.0 5.794382101 1615.0 5.807512383 1686.0 5.820642666 1641.0 5.833772949 1629.0 5.846903231 1646.0 5.860033514 1646.0 5.873163797 1564.0 5.886294079 1569.0 5.899424362 1654.0 5.912554645 1604.0 5.925684927 1623.0 5.938815210 1646.0 5.951945493 1632.0 5.965075775 1702.0 5.978206058 1609.0 5.991336341 1698.0 6.004466623 1678.0 6.017596906 1587.0 6.030727189 1593.0 6.043857471 1688.0 6.056987754 1706.0 6.070118037 1617.0 6.083248319 1607.0 6.096378602 1638.0 6.109508885 1593.0 6.122639168 1590.0 6.135769450 1641.0 6.148899733 1723.0 6.162030016 1723.0 6.175160298 1677.0 6.188290581 1652.0 6.201420864 1619.0 6.214551146 1658.0 6.227681429 1655.0 6.240811712 1634.0 6.253941994 1738.0 6.267072277 1674.0 6.280202560 1717.0 6.293332842 1700.0 6.306463125 1695.0 6.319593408 1628.0 6.332723690 1634.0 6.345853973 1651.0 6.358984256 1667.0 6.372114538 1629.0 6.385244821 1629.0 6.398375104 1696.0 6.411505386 1667.0 6.424635669 1745.0 6.437765952 1715.0 6.450896234 1635.0 6.464026517 1559.0 6.477156800 1610.0 6.490287082 1669.0 6.503417365 1656.0 6.516547648 1621.0 6.529677930 1651.0 6.542808213 1655.0 6.555938496 1645.0 6.569068779 1618.0 6.582199061 1635.0 6.595329344 1743.0 6.608459627 1648.0 6.621589909 1680.0 6.634720192 1698.0 6.647850475 1691.0 6.660980757 1667.0 6.674111040 1680.0 6.687241323 1713.0 6.700371605 1740.0 6.713501888 1666.0 6.726632171 1794.0 6.739762453 1661.0 6.752892736 1614.0 6.766023019 1721.0 6.779153301 1635.0 6.792283584 1702.0 6.805413867 1682.0 6.818544149 1757.0 6.831674432 1706.0 6.844804715 1711.0 6.857934997 1722.0 6.871065280 1736.0 6.884195563 1571.0 6.897325845 1565.0 6.910456128 1666.0 6.923586411 1738.0 6.936716693 1660.0 6.949846976 1671.0 6.962977259 1703.0 6.976107541 1661.0 6.989237824 1771.0 7.002368107 1717.0 7.015498390 1719.0 7.028628672 1674.0 7.041758955 1735.0 7.054889238 1744.0 7.068019520 1727.0 7.081149803 1753.0 7.094280086 1802.0 7.107410368 1734.0 7.120540651 1729.0 7.133670934 1714.0 7.146801216 1711.0 7.159931499 1751.0 7.173061782 1715.0 7.186192064 1707.0 7.199322347 1738.0 7.212452630 1776.0 7.225582912 1661.0 7.238713195 1850.0 7.251843478 1702.0 7.264973760 1757.0 7.278104043 1737.0 7.291234326 1742.0 7.304364608 1728.0 7.317494891 1801.0 7.330625174 1778.0 7.343755456 1740.0 7.356885739 1692.0 7.370016022 1743.0 7.383146304 1764.0 7.396276587 1828.0 7.409406870 1829.0 7.422537152 1807.0 7.435667435 1856.0 7.448797718 1906.0 7.461928001 1820.0 7.475058283 1849.0 7.488188566 1961.0 7.501318849 1910.0 7.514449131 1903.0 7.527579414 1965.0 7.540709697 1893.0 7.553839979 1942.0 7.566970262 2002.0 7.580100545 1998.0 7.593230827 2084.0 7.606361110 2122.0 7.619491393 2100.0 7.632621675 2092.0 7.645751958 2235.0 7.658882241 2177.0 7.672012523 2160.0 7.685142806 2299.0 7.698273089 2317.0 7.711403371 2283.0 7.724533654 2397.0 7.737663937 2492.0 7.750794219 2573.0 7.763924502 2671.0 7.777054785 2760.0 7.790185067 2872.0 7.803315350 2950.0 7.816445633 3086.0 7.829575915 3287.0 7.842706198 3483.0 7.855836481 3721.0 7.868966763 3988.0 7.882097046 4253.0 7.895227329 4253.0 7.908357612 4197.0 7.921487894 3890.0 7.934618177 3598.0 7.947748460 3173.0 7.960878742 2723.0 7.974009025 2330.0 7.987139308 2167.0 8.000269590 1942.0 8.013399873 1958.0 8.026530156 1759.0 8.039660438 1868.0 8.052790721 1789.0 8.065921004 1757.0 8.079051286 1774.0 8.092181569 1722.0 8.105311852 1752.0 8.118442134 1735.0 8.131572417 1702.0 8.144702700 1771.0 8.157832982 1744.0 8.170963265 1765.0 8.184093548 1804.0 8.197223830 1706.0 8.210354113 1758.0 8.223484396 1727.0 8.236614678 1769.0 8.249744961 1672.0 8.262875244 1706.0 8.276005526 1740.0 8.289135809 1706.0 8.302266092 1743.0 8.315396375 1682.0 8.328526657 1719.0 8.341656940 1788.0 8.354787223 1800.0 8.367917505 1862.0 8.381047788 1786.0 8.394178071 1780.0 8.407308353 1843.0 8.420438636 1796.0 8.433568919 1881.0 8.446699201 1795.0 8.459829484 1804.0 8.472959767 1804.0 8.486090049 1835.0 8.499220332 1911.0 8.512350615 1837.0 8.525480897 1919.0 8.538611180 1879.0 8.551741463 2038.0 8.564871745 2033.0 8.578002028 2021.0 8.591132311 2115.0 8.604262593 2142.0 8.617392876 2241.0 8.630523159 2195.0 8.643653441 2268.0 8.656783724 2197.0 8.669914007 2242.0 8.683044289 2313.0 8.696174572 2208.0 8.709304855 2198.0 8.722435137 2084.0 8.735565420 1943.0 8.748695703 1925.0 8.761825986 1770.0 8.774956268 1659.0 8.788086551 1768.0 8.801216834 1720.0 8.814347116 1742.0 8.827477399 1731.0 8.840607682 1752.0 8.853737964 1710.0 8.866868247 1675.0 8.879998530 1701.0 8.893128812 1695.0 8.906259095 1751.0 8.919389378 1578.0 8.932519660 1632.0 8.945649943 1679.0 8.958780226 1684.0 8.971910508 1594.0 8.985040791 1679.0 8.998171074 1577.0 9.011301356 1637.0 9.024431639 1645.0 9.037561922 1673.0 9.050692204 1673.0 9.063822487 1689.0 9.076952770 1732.0 9.090083052 1680.0 9.103213335 1733.0 9.116343618 1589.0 9.129473900 1629.0 9.142604183 1650.0 9.155734466 1639.0 9.168864748 1603.0 9.181995031 1659.0 9.195125314 1680.0 9.208255597 1606.0 9.221385879 1528.0 9.234516162 1668.0 9.247646445 1725.0 9.260776727 1702.0 9.273907010 1723.0 9.287037293 1691.0 9.300167575 1672.0 9.313297858 1699.0 9.326428141 1623.0 9.339558423 1616.0 9.352688706 1574.0 9.365818989 1659.0 9.378949271 1639.0 9.392079554 1569.0 9.405209837 1634.0 9.418340119 1619.0 9.431470402 1675.0 9.444600685 1539.0 9.457730967 1621.0 9.470861250 1575.0 9.483991533 1659.0 9.497121815 1605.0 9.510252098 1637.0 9.523382381 1695.0 9.536512663 1533.0 9.549642946 1650.0 9.562773229 1594.0 9.575903511 1620.0 9.589033794 1509.0 9.602164077 1550.0 9.615294359 1618.0 9.628424642 1619.0 9.641554925 1497.0 9.654685208 1581.0 9.667815490 1618.0 9.680945773 1564.0 9.694076056 1629.0 9.707206338 1525.0 9.720336621 1614.0 9.733466904 1611.0 9.746597186 1648.0 9.759727469 1616.0 9.772857752 1561.0 9.785988034 1568.0 9.799118317 1541.0 9.812248600 1599.0 9.825378882 1438.0 9.838509165 1523.0 9.851639448 1536.0 9.864769730 1547.0 9.877900013 1549.0 9.891030296 1581.0 9.904160578 1631.0 9.917290861 1597.0 9.930421144 1493.0 9.943551426 1628.0 9.956681709 1560.0 9.969811992 1573.0 9.982942274 1575.0 9.996072557 1557.0 10.009202840 1488.0 10.022333122 1549.0 10.035463405 1598.0 10.048593688 1538.0 10.061723970 1536.0 10.074854253 1576.0 10.087984536 1575.0 10.101114819 1504.0 10.114245101 1455.0 10.127375384 1584.0 10.140505667 1620.0 10.153635949 1572.0 10.166766232 1549.0 10.179896515 1488.0 10.193026797 1507.0 10.206157080 1486.0 10.219287363 1552.0 10.232417645 1513.0 10.245547928 1495.0 10.258678211 1545.0 10.271808493 1517.0 10.284938776 1507.0 10.298069059 1471.0 10.311199341 1513.0 10.324329624 1562.0 10.337459907 1477.0 10.350590189 1538.0 10.363720472 1534.0 10.376850755 1499.0 10.389981037 1522.0 10.403111320 1559.0 10.416241603 1519.0 10.429371885 1492.0 10.442502168 1508.0 10.455632451 1500.0 10.468762733 1438.0 10.481893016 1490.0 10.495023299 1495.0 10.508153581 1483.0 10.521283864 1519.0 10.534414147 1529.0 10.547544430 1458.0 10.560674712 1478.0 10.573804995 1521.0 10.586935278 1445.0 10.600065560 1520.0 10.613195843 1430.0 10.626326126 1379.0 10.639456408 1487.0 10.652586691 1490.0 10.665716974 1452.0 10.678847256 1461.0 10.691977539 1470.0 10.705107822 1368.0 10.718238104 1399.0 10.731368387 1457.0 10.744498670 1447.0 10.757628952 1467.0 10.770759235 1451.0 10.783889518 1461.0 10.797019800 1512.0 10.810150083 1397.0 10.823280366 1451.0 10.836410648 1377.0 10.849540931 1446.0 10.862671214 1466.0 10.875801496 1361.0 10.888931779 1433.0 10.902062062 1399.0 10.915192344 1454.0 10.928322627 1382.0 10.941452910 1536.0 10.954583192 1471.0 10.967713475 1356.0 10.980843758 1385.0 10.993974041 1451.0 11.007104323 1491.0 11.020234606 1480.0 11.033364889 1461.0 11.046495171 1390.0 11.059625454 1468.0 11.072755737 1460.0 11.085886019 1493.0 11.099016302 1452.0 11.112146585 1396.0 11.125276867 1444.0 11.138407150 1473.0 11.151537433 1460.0 11.164667715 1438.0 11.177797998 1455.0 11.190928281 1523.0 11.204058563 1462.0 11.217188846 1492.0 11.230319129 1478.0 11.243449411 1500.0 11.256579694 1489.0 11.269709977 1554.0 11.282840259 1548.0 11.295970542 1583.0 11.309100825 1600.0 11.322231107 1594.0 11.335361390 1634.0 11.348491673 1684.0 11.361621955 1710.0 11.374752238 1695.0 11.387882521 1788.0 11.401012803 1761.0 11.414143086 1815.0 11.427273369 1869.0 11.440403652 1899.0 11.453533934 1969.0 11.466664217 1985.0 11.479794500 2078.0 11.492924782 2155.0 11.506055065 2299.0 11.519185348 2435.0 11.532315630 2545.0 11.545445913 2572.0 11.558576196 2755.0 11.571706478 2832.0 11.584836761 2994.0 11.597967044 3292.0 11.611097326 3555.0 11.624227609 3775.0 11.637357892 3994.0 11.650488174 4482.0 11.663618457 4849.0 11.676748740 5294.0 11.689879022 5653.0 11.703009305 6103.0 11.716139588 6385.0 11.729269870 6243.0 11.742400153 6101.0 11.755530436 5472.0 11.768660718 4914.0 11.781791001 4007.0 11.794921284 3197.0 11.808051566 2683.0 11.821181849 2185.0 11.834312132 1941.0 11.847442415 1810.0 11.860572697 1669.0 11.873702980 1670.0 11.886833263 1639.0 11.899963545 1628.0 11.913093828 1555.0 11.926224111 1433.0 11.939354393 1527.0 11.952484676 1464.0 11.965614959 1419.0 11.978745241 1473.0 11.991875524 1400.0 12.005005807 1387.0 12.018136089 1412.0 12.031266372 1390.0 12.044396655 1364.0 12.057526937 1453.0 12.070657220 1330.0 12.083787503 1297.0 12.096917785 1321.0 12.110048068 1347.0 12.123178351 1276.0 12.136308633 1280.0 12.149438916 1384.0 12.162569199 1358.0 12.175699481 1308.0 12.188829764 1369.0 12.201960047 1365.0 12.215090329 1326.0 12.228220612 1361.0 12.241350895 1321.0 12.254481177 1269.0 12.267611460 1281.0 12.280741743 1280.0 12.293872026 1272.0 12.307002308 1323.0 12.320132591 1318.0 12.333262874 1302.0 12.346393156 1327.0 12.359523439 1304.0 12.372653722 1301.0 12.385784004 1309.0 12.398914287 1319.0 12.412044570 1322.0 12.425174852 1280.0 12.438305135 1267.0 12.451435418 1249.0 12.464565700 1300.0 12.477695983 1342.0 12.490826266 1291.0 12.503956548 1354.0 12.517086831 1318.0 12.530217114 1277.0 12.543347396 1295.0 12.556477679 1331.0 12.569607962 1286.0 12.582738244 1289.0 12.595868527 1329.0 12.608998810 1266.0 12.622129092 1239.0 12.635259375 1313.0 12.648389658 1270.0 12.661519940 1338.0 12.674650223 1325.0 12.687780506 1289.0 12.700910788 1238.0 12.714041071 1242.0 12.727171354 1294.0 12.740301637 1316.0 12.753431919 1280.0 12.766562202 1225.0 12.779692485 1273.0 12.792822767 1270.0 12.805953050 1302.0 12.819083333 1266.0 12.832213615 1272.0 12.845343898 1222.0 12.858474181 1263.0 12.871604463 1231.0 12.884734746 1264.0 12.897865029 1255.0 12.910995311 1258.0 12.924125594 1250.0 12.937255877 1193.0 12.950386159 1241.0 12.963516442 1221.0 12.976646725 1192.0 12.989777007 1154.0 13.002907290 1155.0 13.016037573 1291.0 13.029167855 1203.0 13.042298138 1329.0 13.055428421 1225.0 13.068558703 1200.0 13.081688986 1172.0 13.094819269 1194.0 13.107949551 1273.0 13.121079834 1161.0 13.134210117 1190.0 13.147340399 1231.0 13.160470682 1226.0 13.173600965 1216.0 13.186731248 1249.0 13.199861530 1189.0 13.212991813 1241.0 13.226122096 1271.0 13.239252378 1262.0 13.252382661 1263.0 13.265512944 1203.0 13.278643226 1180.0 13.291773509 1343.0 13.304903792 1281.0 13.318034074 1278.0 13.331164357 1336.0 13.344294640 1375.0 13.357424922 1377.0 13.370555205 1323.0 13.383685488 1328.0 13.396815770 1420.0 13.409946053 1419.0 13.423076336 1436.0 13.436206618 1487.0 13.449336901 1505.0 13.462467184 1579.0 13.475597466 1670.0 13.488727749 1677.0 13.501858032 1788.0 13.514988314 1827.0 13.528118597 1983.0 13.541248880 1910.0 13.554379162 2080.0 13.567509445 2159.0 13.580639728 2372.0 13.593770010 2584.0 13.606900293 2801.0 13.620030576 2899.0 13.633160859 3327.0 13.646291141 3577.0 13.659421424 3988.0 13.672551707 4141.0 13.685681989 4179.0 13.698812272 4188.0 13.711942555 3661.0 13.725072837 3232.0 13.738203120 2742.0 13.751333403 2166.0 13.764463685 1781.0 13.777593968 1541.0 13.790724251 1450.0 13.803854533 1366.0 13.816984816 1242.0 13.830115099 1244.0 13.843245381 1252.0 13.856375664 1213.0 13.869505947 1203.0 13.882636229 1168.0 13.895766512 1208.0 13.908896795 1196.0 13.922027077 1212.0 13.935157360 1119.0 13.948287643 1117.0 13.961417925 1227.0 13.974548208 1132.0 13.987678491 1174.0 14.000808773 1161.0 14.013939056 1161.0 14.027069339 1084.0 14.040199621 1105.0 14.053329904 1170.0 14.066460187 1144.0 14.079590470 1149.0 14.092720752 1120.0 14.105851035 1129.0 14.118981318 1087.0 14.132111600 1177.0 14.145241883 1119.0 14.158372166 1103.0 14.171502448 1093.0 14.184632731 1126.0 14.197763014 1180.0 14.210893296 1105.0 14.224023579 1153.0 14.237153862 1090.0 14.250284144 1059.0 14.263414427 1093.0 14.276544710 1102.0 14.289674992 1141.0 14.302805275 1089.0 14.315935558 1097.0 14.329065840 1108.0 14.342196123 1092.0 14.355326406 1086.0 14.368456688 1079.0 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