ECNU-21,calcined Rigaku Ultima IV X-ray diffractometer Wavelength: CuK(alpha) 1.5406 Å ----- 7.00127 560.04000 7.00941 556.68000 7.01754 537.60000 7.02568 583.61000 7.03381 575.76000 7.04195 549.94000 7.05008 571.83000 7.05822 523.01000 7.06635 571.27000 7.07449 548.26000 7.08262 537.04000 7.09076 551.07000 7.09889 539.84000 7.10703 521.32000 7.11516 591.47000 7.12330 545.45000 7.13143 594.84000 7.13957 563.41000 7.14770 554.43000 7.15584 549.94000 7.16397 558.92000 7.17211 572.39000 7.18024 593.15000 7.18838 582.49000 7.19651 601.57000 7.20465 590.35000 7.21278 571.27000 7.22091 616.72000 7.22905 597.64000 7.23718 588.10000 7.24532 592.59000 7.25345 562.29000 7.26159 584.18000 7.26972 579.12000 7.27786 553.31000 7.28599 547.70000 7.29413 543.21000 7.30226 544.89000 7.31040 554.43000 7.31853 543.21000 7.32667 514.03000 7.33480 536.48000 7.34294 537.04000 7.35107 533.67000 7.35921 573.51000 7.36734 540.40000 7.37548 512.91000 7.38361 558.36000 7.39175 540.40000 7.39988 546.58000 7.40802 539.84000 7.41615 538.16000 7.42429 550.51000 7.43242 544.33000 7.44056 547.14000 7.44869 540.97000 7.45683 539.84000 7.46496 572.95000 7.47310 562.29000 7.48123 557.24000 7.48936 570.15000 7.49750 524.13000 7.50563 552.19000 7.51377 540.97000 7.52190 571.27000 7.53004 567.34000 7.53817 581.37000 7.54631 547.14000 7.55444 570.71000 7.56258 588.10000 7.57071 586.98000 7.57885 589.23000 7.58698 641.98000 7.59512 608.31000 7.60325 648.15000 7.61139 669.47000 7.61952 662.74000 7.62766 639.73000 7.63579 672.28000 7.64393 714.93000 7.65206 742.42000 7.66020 734.01000 7.66833 696.41000 7.67647 711.56000 7.68460 676.77000 7.69274 659.37000 7.70087 679.01000 7.70901 671.72000 7.71714 676.21000 7.72528 672.84000 7.73341 666.11000 7.74155 646.46000 7.74968 651.52000 7.75782 679.01000 7.76595 653.20000 7.77408 690.24000 7.78222 684.06000 7.79035 643.66000 7.79849 664.42000 7.80662 671.72000 7.81476 643.10000 7.82289 649.27000 7.83103 659.93000 7.83916 657.69000 7.84730 689.11000 7.85543 678.45000 7.86357 693.04000 7.87170 691.36000 7.87984 682.94000 7.88797 695.29000 7.89611 704.26000 7.90424 714.37000 7.91238 751.96000 7.92051 747.47000 7.92865 763.75000 7.93678 789.56000 7.94492 809.20000 7.95305 773.29000 7.96119 826.04000 7.96932 819.87000 7.97746 929.85000 7.98559 882.15000 7.99373 957.91000 8.00186 960.16000 8.01000 1011.22000 8.01813 1104.94000 8.02627 1130.19000 8.03440 1194.73000 8.04253 1268.80000 8.05067 1291.81000 8.05880 1325.48000 8.06694 1469.14000 8.07507 1548.82000 8.08321 1649.27000 8.09134 1682.38000 8.09948 1826.60000 8.10761 1934.90000 8.11575 2081.93000 8.12388 2127.95000 8.13202 2307.52000 8.14015 2554.43000 8.14829 2660.49000 8.15642 2882.15000 8.16456 3069.58000 8.17269 3441.08000 8.18083 3726.15000 8.18896 3998.88000 8.19710 4294.61000 8.20523 4726.71000 8.21337 5110.55000 8.22150 5296.30000 8.22964 5303.03000 8.23777 5025.25000 8.24591 4470.82000 8.25404 3856.34000 8.26218 3220.54000 8.27031 2641.41000 8.27845 2152.64000 8.28658 1806.96000 8.29472 1570.71000 8.30285 1396.75000 8.31098 1253.65000 8.31912 1189.11000 8.32725 1043.77000 8.33539 988.22000 8.34352 897.87000 8.35166 914.14000 8.35979 822.67000 8.36793 823.79000 8.37606 790.12000 8.38420 802.47000 8.39233 754.77000 8.40047 687.43000 8.40860 687.99000 8.41674 704.83000 8.42487 646.46000 8.43301 651.52000 8.44114 653.20000 8.44928 645.90000 8.45741 636.92000 8.46555 632.44000 8.47368 592.59000 8.48182 588.66000 8.48995 601.57000 8.49809 627.95000 8.50622 591.47000 8.51436 621.21000 8.52249 597.64000 8.53063 587.54000 8.53876 554.99000 8.54690 590.91000 8.55503 546.58000 8.56317 554.43000 8.57130 557.24000 8.57944 562.29000 8.58757 590.91000 8.59570 555.56000 8.60384 538.16000 8.61197 572.39000 8.62011 565.66000 8.62824 551.63000 8.63638 556.12000 8.64451 535.91000 8.65265 540.40000 8.66078 507.30000 8.66892 530.86000 8.67705 536.48000 8.68519 516.84000 8.69332 531.99000 8.70146 523.57000 8.70959 519.64000 8.71773 501.68000 8.72586 534.23000 8.73400 505.05000 8.74213 521.89000 8.75027 523.01000 8.75840 515.15000 8.76654 502.24000 8.77467 526.94000 8.78281 494.39000 8.79094 522.45000 8.79908 503.93000 8.80721 518.52000 8.81535 471.94000 8.82348 509.54000 8.83162 511.78000 8.83975 525.81000 8.84789 506.17000 8.85602 475.31000 8.86415 491.02000 8.87229 509.54000 8.88042 492.70000 8.88856 514.03000 8.89669 524.69000 8.90483 527.50000 8.91296 505.05000 8.92110 452.86000 8.92923 488.22000 8.93737 521.32000 8.94550 478.11000 8.95364 493.83000 8.96177 497.76000 8.96991 526.37000 8.97804 512.91000 8.98618 498.32000 8.99431 506.17000 9.00245 506.73000 9.01058 487.65000 9.01872 510.66000 9.02685 504.49000 9.03499 516.27000 9.04312 489.90000 9.05126 502.24000 9.05939 494.95000 9.06753 496.63000 9.07566 502.81000 9.08380 517.40000 9.09193 485.97000 9.10007 493.27000 9.10820 519.64000 9.11634 503.93000 9.12447 476.99000 9.13261 474.75000 9.14074 472.50000 9.14887 495.51000 9.15701 533.11000 9.16514 487.09000 9.17328 489.90000 9.18141 484.29000 9.18955 484.29000 9.19768 507.86000 9.20582 517.40000 9.21395 517.40000 9.22209 491.58000 9.23022 475.87000 9.23836 498.88000 9.24649 541.53000 9.25463 526.94000 9.26276 489.90000 9.27090 501.68000 9.27903 501.12000 9.28717 482.04000 9.29530 505.61000 9.30344 515.15000 9.31157 502.81000 9.31971 506.17000 9.32784 515.15000 9.33598 539.28000 9.34411 535.91000 9.35225 518.52000 9.36038 525.81000 9.36852 531.99000 9.37665 530.30000 9.38479 503.37000 9.39292 524.13000 9.40106 533.11000 9.40919 516.27000 9.41732 526.94000 9.42546 549.38000 9.43359 535.35000 9.44173 538.72000 9.44986 523.57000 9.45800 531.99000 9.46613 534.23000 9.47427 544.33000 9.48240 534.23000 9.49054 568.46000 9.49867 536.48000 9.50681 550.51000 9.51494 526.94000 9.52308 565.66000 9.53121 569.02000 9.53935 541.53000 9.54748 591.47000 9.55562 602.69000 9.56375 567.34000 9.57189 556.12000 9.58002 580.81000 9.58816 535.91000 9.59629 562.85000 9.60443 553.31000 9.61256 604.94000 9.62070 603.82000 9.62883 583.61000 9.63697 612.23000 9.64510 625.70000 9.65324 607.18000 9.66137 575.76000 9.66951 606.62000 9.67764 590.35000 9.68577 575.76000 9.69391 589.23000 9.70204 628.51000 9.71018 630.75000 9.71831 651.52000 9.72645 629.63000 9.73458 657.69000 9.74272 642.54000 9.75085 686.87000 9.75899 674.52000 9.76712 640.85000 9.77526 679.01000 9.78339 629.63000 9.79153 660.49000 9.79966 672.28000 9.80780 664.98000 9.81593 686.87000 9.82407 697.53000 9.83220 679.01000 9.84034 675.08000 9.84847 725.03000 9.85661 727.27000 9.86474 709.32000 9.87288 736.25000 9.88101 767.12000 9.88915 763.19000 9.89728 759.82000 9.90542 728.40000 9.91355 838.95000 9.92169 769.36000 9.92982 790.12000 9.93796 805.84000 9.94609 847.92000 9.95423 902.36000 9.96236 895.62000 9.97049 898.43000 9.97863 903.48000 9.98676 945.01000 9.99490 968.01000 10.00303 996.63000 10.01117 1051.07000 10.01930 1044.33000 10.02744 1111.67000 10.03557 1134.68000 10.04371 1147.03000 10.05184 1193.04000 10.05998 1221.10000 10.06811 1293.49000 10.07625 1382.72000 10.08438 1464.65000 10.09252 1551.07000 10.10065 1610.55000 10.10879 1761.50000 10.11692 1870.37000 10.12506 1957.35000 10.13319 2166.11000 10.14133 2343.43000 10.14946 2462.96000 10.15760 2683.50000 10.16573 2832.77000 10.17387 3047.14000 10.18200 3368.69000 10.19014 3697.53000 10.19827 4033.67000 10.20641 4393.38000 10.21454 4818.74000 10.22268 5257.58000 10.23081 5773.29000 10.23894 6349.61000 10.24708 7007.30000 10.25521 7605.50000 10.26335 8167.23000 10.27148 8724.47000 10.27962 9188.55000 10.28775 9751.40000 10.29589 9877.10000 10.30402 9893.38000 10.31216 9466.33000 10.32029 8884.96000 10.32843 8037.04000 10.33656 6877.10000 10.34470 5964.09000 10.35283 5086.42000 10.36097 4290.12000 10.36910 3749.72000 10.37724 3287.88000 10.38537 2774.97000 10.39351 2348.48000 10.40164 2154.88000 10.40978 2030.86000 10.41791 1710.44000 10.42605 1619.53000 10.43418 1462.96000 10.44232 1433.22000 10.45045 1364.20000 10.45859 1204.83000 10.46672 1166.67000 10.47486 1111.67000 10.48299 1035.91000 10.49113 1034.23000 10.49926 939.96000 10.50740 931.54000 10.51553 861.39000 10.52366 849.61000 10.53180 835.58000 10.53993 818.18000 10.54807 792.93000 10.55620 757.58000 10.56434 730.08000 10.57247 684.06000 10.58061 708.75000 10.58874 687.99000 10.59688 684.06000 10.60501 648.15000 10.61315 703.14000 10.62128 648.15000 10.62942 631.31000 10.63755 645.90000 10.64569 610.55000 10.65382 623.46000 10.66196 608.87000 10.67009 596.52000 10.67823 568.46000 10.68636 611.11000 10.69450 556.12000 10.70263 542.09000 10.71077 569.58000 10.71890 569.02000 10.72704 544.89000 10.73517 562.85000 10.74331 546.02000 10.75144 524.13000 10.75958 553.87000 10.76771 538.16000 10.77585 519.08000 10.78398 552.75000 10.79211 527.50000 10.80025 497.76000 10.80838 501.68000 10.81652 497.19000 10.82465 525.25000 10.83279 535.35000 10.84092 535.91000 10.84906 517.40000 10.85719 510.66000 10.86533 515.71000 10.87346 495.51000 10.88160 506.73000 10.88973 491.58000 10.89787 487.09000 10.90600 482.60000 10.91414 487.09000 10.92227 476.99000 10.93041 477.55000 10.93854 494.39000 10.94668 471.38000 10.95481 482.60000 10.96295 498.88000 10.97108 502.24000 10.97922 491.02000 10.98735 496.63000 10.99549 462.96000 11.00362 471.38000 11.01176 468.57000 11.01989 459.03000 11.02803 474.75000 11.03616 481.48000 11.04430 484.85000 11.05243 474.19000 11.06056 475.31000 11.06870 456.79000 11.07683 469.14000 11.08497 462.96000 11.09310 459.60000 11.10124 443.32000 11.10937 450.62000 11.11751 445.01000 11.12564 480.92000 11.13378 456.23000 11.14191 459.60000 11.15005 493.83000 11.15818 451.18000 11.16632 468.01000 11.17445 477.55000 11.18259 447.81000 11.19072 476.99000 11.19886 446.13000 11.20699 445.01000 11.21513 466.33000 11.22326 427.61000 11.23140 436.59000 11.23953 432.66000 11.24767 440.52000 11.25580 454.55000 11.26394 430.98000 11.27207 440.52000 11.28021 455.11000 11.28834 442.20000 11.29648 436.03000 11.30461 460.72000 11.31275 463.52000 11.32088 441.08000 11.32902 476.99000 11.33715 434.34000 11.34528 415.26000 11.35342 441.64000 11.36155 411.90000 11.36969 420.31000 11.37782 460.16000 11.38596 428.73000 11.39409 434.90000 11.40223 446.13000 11.41036 428.73000 11.41850 441.64000 11.42663 452.86000 11.43477 429.29000 11.44290 440.52000 11.45104 413.02000 11.45917 438.83000 11.46731 414.70000 11.47544 420.88000 11.48358 443.32000 11.49171 453.98000 11.49985 429.29000 11.50798 452.30000 11.51612 447.81000 11.52425 436.59000 11.53239 462.96000 11.54052 418.07000 11.54866 448.93000 11.55679 425.93000 11.56493 429.29000 11.57306 434.90000 11.58120 413.58000 11.58933 447.81000 11.59747 445.57000 11.60560 412.46000 11.61373 439.39000 11.62187 441.64000 11.63000 427.05000 11.63814 428.73000 11.64627 436.03000 11.65441 450.06000 11.66254 442.76000 11.67068 447.25000 11.67881 446.69000 11.68695 455.11000 11.69508 458.47000 11.70322 423.12000 11.71135 447.81000 11.71949 458.47000 11.72762 420.88000 11.73576 417.51000 11.74389 423.68000 11.75203 424.24000 11.76016 437.15000 11.76830 436.03000 11.77643 425.93000 11.78457 428.17000 11.79270 416.95000 11.80084 428.73000 11.80897 435.47000 11.81711 430.42000 11.82524 398.99000 11.83338 435.47000 11.84151 430.42000 11.84965 408.53000 11.85778 393.38000 11.86592 405.16000 11.87405 433.78000 11.88219 411.90000 11.89032 423.12000 11.89845 468.01000 11.90659 413.58000 11.91472 441.64000 11.92286 434.34000 11.93099 426.49000 11.93913 432.10000 11.94726 460.72000 11.95540 427.05000 11.96353 432.66000 11.97167 447.25000 11.97980 432.10000 11.98794 409.65000 11.99607 404.60000 12.00421 430.98000 12.01234 439.39000 12.02048 438.83000 12.02861 407.41000 12.03675 461.84000 12.04488 424.24000 12.05302 415.26000 12.06115 451.18000 12.06929 416.39000 12.07742 425.36000 12.08556 436.03000 12.09369 434.34000 12.10183 411.90000 12.10996 415.26000 12.11810 409.09000 12.12623 434.34000 12.13437 438.83000 12.14250 463.52000 12.15064 410.21000 12.15877 405.16000 12.16690 461.84000 12.17504 409.65000 12.18317 420.88000 12.19131 420.31000 12.19944 446.13000 12.20758 454.55000 12.21571 426.49000 12.22385 443.32000 12.23198 430.98000 12.24012 421.44000 12.24825 428.73000 12.25639 437.71000 12.26452 420.88000 12.27266 438.83000 12.28079 404.04000 12.28893 451.18000 12.29706 410.21000 12.30520 428.73000 12.31333 434.90000 12.32147 441.08000 12.32960 451.74000 12.33774 414.14000 12.34587 439.39000 12.35401 426.49000 12.36214 420.88000 12.37028 465.21000 12.37841 451.74000 12.38655 435.47000 12.39468 448.93000 12.40282 437.15000 12.41095 461.84000 12.41909 453.98000 12.42722 451.74000 12.43536 421.44000 12.44349 434.34000 12.45162 423.12000 12.45976 452.30000 12.46789 471.94000 12.47603 433.22000 12.48416 455.67000 12.49230 488.22000 12.50043 466.89000 12.50857 442.76000 12.51670 434.34000 12.52484 460.72000 12.53297 453.98000 12.54111 468.01000 12.54924 473.06000 12.55738 475.31000 12.56551 487.09000 12.57365 468.57000 12.58178 500.56000 12.58992 497.76000 12.59805 507.86000 12.60619 506.17000 12.61432 520.20000 12.62246 522.45000 12.63059 523.01000 12.63873 531.43000 12.64686 529.18000 12.65500 585.86000 12.66313 574.07000 12.67127 626.82000 12.67940 672.28000 12.68754 681.82000 12.69567 709.32000 12.70381 758.14000 12.71194 836.70000 12.72007 867.00000 12.72821 985.41000 12.73634 1045.45000 12.74448 1138.61000 12.75261 1263.75000 12.76075 1412.46000 12.76888 1625.14000 12.77702 1869.81000 12.78515 2099.33000 12.79329 2396.75000 12.80142 2823.23000 12.80956 3296.30000 12.81769 3876.54000 12.82583 4535.91000 12.83396 5218.29000 12.84210 6337.26000 12.85023 7402.92000 12.85837 8461.28000 12.86650 9156.57000 12.87464 9092.03000 12.88277 8509.54000 12.89091 7467.45000 12.89904 6235.69000 12.90718 4813.69000 12.91531 3851.85000 12.92345 3084.18000 12.93158 2525.25000 12.93972 2121.21000 12.94785 1824.35000 12.95599 1624.58000 12.96412 1424.24000 12.97226 1317.62000 12.98039 1213.80000 12.98852 1073.51000 12.99666 1076.88000 13.00479 951.18000 13.01293 895.06000 13.02106 842.87000 13.02920 810.89000 13.03733 709.32000 13.04547 696.41000 13.05360 687.43000 13.06174 676.77000 13.06987 647.59000 13.07801 637.49000 13.08614 594.84000 13.09428 579.12000 13.10241 571.83000 13.11055 548.82000 13.11868 542.09000 13.12682 530.30000 13.13495 525.25000 13.14309 534.23000 13.15122 513.47000 13.15936 497.76000 13.16749 491.02000 13.17563 497.76000 13.18376 508.42000 13.19190 515.15000 13.20003 503.37000 13.20817 514.03000 13.21630 484.29000 13.22444 507.86000 13.23257 495.51000 13.24071 480.92000 13.24884 496.63000 13.25698 481.48000 13.26511 476.43000 13.27324 489.90000 13.28138 463.52000 13.28951 457.91000 13.29765 518.52000 13.30578 484.29000 13.31392 461.28000 13.32205 459.03000 13.33019 463.52000 13.33832 449.49000 13.34646 462.96000 13.35459 449.49000 13.36273 460.72000 13.37086 464.09000 13.37900 456.79000 13.38713 481.48000 13.39527 451.74000 13.40340 442.20000 13.41154 453.98000 13.41967 452.86000 13.42781 463.52000 13.43594 456.79000 13.44408 434.90000 13.45221 471.38000 13.46035 452.30000 13.46848 443.32000 13.47662 459.03000 13.48475 439.39000 13.49289 451.74000 13.50102 419.75000 13.50916 446.13000 13.51729 462.40000 13.52543 446.13000 13.53356 468.57000 13.54169 452.86000 13.54983 441.08000 13.55796 427.05000 13.56610 429.29000 13.57423 438.83000 13.58237 432.10000 13.59050 455.11000 13.59864 438.27000 13.60677 467.45000 13.61491 442.20000 13.62304 426.49000 13.63118 433.22000 13.63931 417.51000 13.64745 422.56000 13.65558 420.88000 13.66372 432.66000 13.67185 450.06000 13.67999 462.96000 13.68812 417.51000 13.69626 410.77000 13.70439 435.47000 13.71253 458.47000 13.72066 460.16000 13.72880 392.26000 13.73693 437.71000 13.74507 441.64000 13.75320 448.37000 13.76134 437.71000 13.76947 447.25000 13.77761 444.44000 13.78574 409.65000 13.79388 418.63000 13.80201 438.27000 13.81015 431.54000 13.81828 411.90000 13.82641 455.67000 13.83455 434.34000 13.84268 419.75000 13.85082 455.11000 13.85895 431.54000 13.86709 436.59000 13.87522 443.88000 13.88336 422.56000 13.89149 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