data_1_publ

_pd_block_id
  2018-07-25T12:51|1||

_audit_creation_method  "from EXP file using GSAS2CIF"
_audit_creation_date                   2018-07-25T12:51
_audit_author_name                     ""
_audit_update_record
; 2018-07-25T12:51  Initial CIF as created by GSAS2CIF
;

#=============================================================================
# this information describes the project, paper etc. for the CIF             #
# Acta Cryst. Section C papers and editorial correspondence is generated     #
# from the information in this section                                       #
#                                                                            #
#   (from)   CIF submission form for Rietveld refinements (Acta Cryst. C)    #
#                                                 Version 14 December 1998   #
#=============================================================================
# 1. SUBMISSION DETAILS

_publ_contact_author_name            ?   # Name of author for correspondence
_publ_contact_author_address             # Address of author for correspondence
; ?
;
_publ_contact_author_email           ?
_publ_contact_author_fax             ?
_publ_contact_author_phone           ?

_publ_contact_letter
; ?
;

_publ_requested_journal              ?
_publ_requested_coeditor_name        ?
_publ_requested_category             ?   # Acta C: one of CI/CM/CO/FI/FM/FO

#==============================================================================

# 2. PROCESSING SUMMARY (IUCr Office Use Only)

_journal_data_validation_number      ?

_journal_date_recd_electronic        ?
_journal_date_to_coeditor            ?
_journal_date_from_coeditor          ?
_journal_date_accepted               ?
_journal_date_printers_first         ?
_journal_date_printers_final         ?
_journal_date_proofs_out             ?
_journal_date_proofs_in              ?
_journal_coeditor_name               ?
_journal_coeditor_code               ?
_journal_coeditor_notes
; ?
;
_journal_techeditor_code             ?
_journal_techeditor_notes
; ?
;
_journal_coden_ASTM                  ?
_journal_name_full                   ?
_journal_year                        ?
_journal_volume                      ?
_journal_issue                       ?
_journal_page_first                  ?
_journal_page_last                   ?
_journal_paper_category              ?
_journal_suppl_publ_number           ?
_journal_suppl_publ_pages            ?

#==============================================================================

# 3. TITLE AND AUTHOR LIST

_publ_section_title
; ?
;
_publ_section_title_footnote
; ?
;

# The loop structure below should contain the names and addresses of all
# authors, in the required order of publication. Repeat as necessary.

loop_
	_publ_author_name
        _publ_author_footnote
	_publ_author_address
 ?                                   #<--'Last name, first name'
; ?
;
; ?
;

#==============================================================================

# 4. TEXT

_publ_section_synopsis
;  ?
;
_publ_section_abstract
; ?
;
_publ_section_comment
; ?
;
_publ_section_exptl_prep      # Details of the preparation of the sample(s)
                              # should be given here.
; ?
;
_publ_section_exptl_refinement
; ?
;
_publ_section_references
; ?
;
_publ_section_figure_captions
; ?
;
_publ_section_acknowledgements
; ?
;

#=============================================================================
# 5. OVERALL REFINEMENT & COMPUTING DETAILS

_refine_special_details
; ?
;
_pd_proc_ls_special_details
; ?
;

# The following items are used to identify the programs used.
_computing_molecular_graphics     ?
_computing_publication_material   ?

_refine_ls_weighting_scheme       ?
_refine_ls_weighting_details      ?
_refine_ls_hydrogen_treatment     ?
_refine_ls_extinction_method      ?
_refine_ls_extinction_coef        ?
_refine_ls_number_constraints     ?

_refine_ls_restrained_S_all       ?
_refine_ls_restrained_S_obs       ?

#==============================================================================
# 6. SAMPLE PREPARATION DATA

# (In the unusual case where multiple samples are used in a single
#  Rietveld study, this information should be moved into the phase
#  blocks)

# The following three fields describe the preparation of the material.
# The cooling rate is in K/min.  The pressure at which the sample was
# prepared is in kPa.  The temperature of preparation is in K.

_pd_prep_cool_rate                ?
_pd_prep_pressure                 ?
_pd_prep_temperature              ?

_pd_char_colour                   ?       # use ICDD colour descriptions
_refine_ls_shift/su_max                0.22
_refine_ls_shift/su_mean               0.03
_computing_structure_refinement        GSAS
_refine_ls_number_parameters           143
_refine_ls_goodness_of_fit_all         3.77
_refine_ls_number_restraints           94
_refine_ls_matrix_type                 full
#==============================================================================
# 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA

_pd_char_particle_morphology      ?

_chemical_name_systematic
; ?
;
_chemical_name_common             ?
_chemical_formula_moiety          ?
_chemical_formula_structural      ?
_chemical_formula_analytical      ?
_chemical_melting_point           ?
_chemical_compound_source         ?       # for minerals and
                                          # natural products
_symmetry_space_group_name_Hall   ?

_exptl_crystal_F_000               ?
_exptl_crystal_density_diffrn      ?
_exptl_crystal_density_meas        ?
_exptl_crystal_density_method      ?

_cell_measurement_temperature     ?

_cell_special_details
; ?
;

_geom_special_details             ?

# The following item identifies the program(s) used (if appropriate).
_computing_structure_solution     ?

#==============================================================================

# 8. Phase information from GSAS

_pd_phase_name                         tetra
_cell_length_a                         14.2913(5)
_cell_length_b                         14.2913
_cell_length_c                         17.9324(14)
_cell_angle_alpha                      90.0
_cell_angle_beta                       90.0
_cell_angle_gamma                      90.0
_cell_volume                           3662.5(4)
_symmetry_cell_setting                 tetragonal
_symmetry_space_group_name_H-M         "P -4 21 c"
loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz
       1 +x,+y,+z 
       2 +y,-x,-z 
       3 -x,-y,+z 
       4 -y,+x,-z 
       5 -x+1/2,+y+1/2,-z+1/2 
       6 +y+1/2,+x+1/2,+z+1/2 
       7 +x+1/2,-y+1/2,-z+1/2 
       8 -y+1/2,-x+1/2,+z+1/2 

# ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS


loop_
      _atom_site_type_symbol
      _atom_site_label
      _atom_site_fract_x
      _atom_site_fract_y
      _atom_site_fract_z
      _atom_site_occupancy
      _atom_site_thermal_displace_type
      _atom_site_U_iso_or_equiv
      _atom_site_symmetry_multiplicity
Al
Al1     0.1001(8)    0.3844(8)    0.4203(7)    1.0        Uiso   0.0125(8)     8
Al
Al2     0.2406(9)    0.2332(9)    0.1611(7)    1.0        Uiso   0.0125(8)     8
Al
Al3     0.2370(9)    0.1096(8)    0.4573(7)    1.0        Uiso   0.0125(8)     8
Al
Al4     0.3777(8)    0.4012(8)    0.4209(7)    1.0        Uiso   0.0125(8)     8
P 
P5      0.2449(7)    0.2703(6)    0.3353(5)    1.0        Uiso   0.0125(8)     8
P 
P6      0.3887(7)    0.1021(6)    0.0717(5)    1.0        Uiso   0.0125(8)     8
P 
P7      0.1059(6)    0.1105(6)    0.0843(5)    1.0        Uiso   0.0125(8)     8
P 
P8      0.2732(7)    0.3938(7)    0.0511(5)    1.0        Uiso   0.0125(8)     8
O 
O9      0.3624(9)   -0.0024(5)    0.0610(8)    1.0        Uiso   0.0283(23)    8
O 
O10     0.1622(6)    0.3366(7)    0.3455(6)    1.0        Uiso   0.0283(23)    8
O 
O11     0.4845(5)    0.1051(9)    0.1099(7)    1.0        Uiso   0.0283(23)    8
O 
O12     0.2011(6)    0.4018(10)  -0.0102(5)    1.0        Uiso   0.0283(23)    8
O 
O13     0.2576(11)   0.2425(10)   0.2547(4)    1.0        Uiso   0.0283(23)    8
O 
O14     0.2409(10)   0.3396(6)    0.1184(5)    1.0        Uiso   0.0283(23)    8
O 
O15     0.3251(6)    0.1578(7)    0.1234(6)    1.0        Uiso   0.0283(23)    8
O 
O16     0.1353(6)    0.1779(7)    0.1450(5)    1.0        Uiso   0.0283(23)    8
O 
O17     0.3333(6)    0.3246(7)    0.3573(6)    1.0        Uiso   0.0283(23)    8
O 
O18     0.2350(11)   0.1834(6)    0.3820(5)    1.0        Uiso   0.0283(23)    8
O 
O19     0.3465(6)    0.1079(11)   0.4974(5)    1.0        Uiso   0.0283(23)    8
O 
O20     1.0002(4)    0.1019(10)   0.0879(8)    1.0        Uiso   0.0283(23)    8
O 
O21     0.1340(9)    0.1484(9)    0.0090(4)    1.0        Uiso   0.0283(23)    8
O 
O22     0.1533(8)    0.0160(5)    0.0955(8)    1.0        Uiso   0.0283(23)    8
O 
O23     0.3612(6)    0.3498(7)    0.0199(6)    1.0        Uiso   0.0283(23)    8
O 
O24     0.2079(9)   -0.0033(5)    0.4253(7)    1.0        Uiso   0.0283(23)    8
 
# If you change Z, be sure to change all 3 of the following
_chemical_formula_sum                  "Al O4 P"
_chemical_formula_weight               121.95
_cell_formula_units_Z                  32

# MOLECULAR GEOMETRY

loop_
      _geom_bond_atom_site_label_1
      _geom_bond_atom_site_label_2
      _geom_bond_distance
      _geom_bond_site_symmetry_1
      _geom_bond_site_symmetry_2
      _geom_bond_publ_flag
  Al1       P5               3.044(15)  .      1_555  N
  Al1       P6               3.031(16)  .      7_455  N
  Al1       O9               1.737(14)  .      5_555  N
  Al1       O10              1.748(16)  .      1_555  N
  Al1       O11              1.745(15)  .      7_455  N
  Al1       O12              1.746(15)  .      8_555  N
  Al2       P7               2.946(15)  .      1_555  N
  Al2       P8               3.062(16)  .      1_555  N
  Al2       O13              1.701(14)  .      1_555  N
  Al2       O14              1.703(15)  .      1_555  N
  Al2       O15              1.754(16)  .      1_555  N
  Al2       O16              1.724(16)  .      1_555  N
  Al3       P8               3.023(16)  .      8_555  N
  Al3       O18              1.713(15)  .      1_555  N
  Al3       O19              1.723(15)  .      1_555  N
  Al3       O23              1.726(16)  .      8_555  N
  Al3       O24              1.763(14)  .      1_555  N
  Al4       P5               3.076(15)  .      1_555  N
  Al4       P7               3.001(14)  .      5_555  N
  Al4       P7               2.937(16)  .      8_555  N
  Al4       O17              1.705(15)  .      1_555  N
  Al4       O20              1.757(13)  .      7_455  N
  Al4       O21              1.699(15)  .      8_555  N
  Al4       O22              1.724(14)  .      5_555  N
  P5        Al1              3.044(15)  .      1_555  N
  P5        Al4              3.076(15)  .      1_555  N
  P5        O10              1.525(13)  .      1_555  N
  P5        O13              1.510(12)  .      1_555  N
  P5        O17              1.534(13)  .      1_555  N
  P5        O18              1.505(12)  .      1_555  N
  P6        Al1              3.031(16)  .      7_555  N
  P6        O9               1.552(11)  .      1_555  N
  P6        O11              1.533(13)  .      1_555  N
  P6        O15              1.523(14)  .      1_555  N
  P6        O19              1.521(12)  .      8_554  N
  P7        Al2              2.946(15)  .      1_555  N
  P7        Al4              3.001(14)  .      5_545  N
  P7        Al4              2.937(16)  .      8_554  N
  P7        O16              1.513(13)  .      1_555  N
  P7        O20              1.518(11)  .      1_455  N
  P7        O21              1.510(12)  .      1_555  N
  P7        O22              1.524(12)  .      1_555  N
  P8        Al2              3.062(16)  .      1_555  N
  P8        Al3              3.023(16)  .      8_554  N
  P8        O12              1.510(13)  .      1_555  N
  P8        O14              1.506(13)  .      1_555  N
  P8        O23              1.514(13)  .      1_555  N
  P8        O24              1.554(13)  .      5_555  N
  O9        Al1              1.737(14)  .      5_545  N
  O9        P6               1.552(11)  .      1_555  N
  O10       Al1              1.748(16)  .      1_555  N
  O10       P5               1.525(13)  .      1_555  N
  O11       Al1              1.745(15)  .      7_555  N
  O11       P6               1.533(13)  .      1_555  N
  O12       Al1              1.746(15)  .      8_554  N
  O12       P8               1.510(13)  .      1_555  N
  O13       Al2              1.701(14)  .      1_555  N
  O13       P5               1.510(12)  .      1_555  N
  O14       Al2              1.703(15)  .      1_555  N
  O14       P8               1.506(13)  .      1_555  N
  O15       Al2              1.754(16)  .      1_555  N
  O15       P6               1.523(14)  .      1_555  N
  O16       Al2              1.724(16)  .      1_555  N
  O16       P7               1.513(13)  .      1_555  N
  O17       Al4              1.705(15)  .      1_555  N
  O17       P5               1.534(13)  .      1_555  N
  O18       Al3              1.713(15)  .      1_555  N
  O18       P5               1.505(12)  .      1_555  N
  O19       Al3              1.723(15)  .      1_555  N
  O19       P6               1.521(12)  .      8_555  N
  O20       Al4              1.757(13)  .      7_555  N
  O20       P7               1.518(11)  .      1_655  N
  O21       Al4              1.699(15)  .      8_554  N
  O21       P7               1.510(12)  .      1_555  N
  O22       Al4              1.724(14)  .      5_545  N
  O22       P7               1.524(12)  .      1_555  N
  O23       Al3              1.726(16)  .      8_554  N
  O23       P8               1.514(13)  .      1_555  N
  O24       Al3              1.763(14)  .      1_555  N
  O24       P8               1.554(13)  .      5_545  N

loop_
      _geom_angle_atom_site_label_1
      _geom_angle_atom_site_label_2
      _geom_angle_atom_site_label_3
      _geom_angle
      _geom_angle_site_symmetry_1
      _geom_angle_site_symmetry_2
      _geom_angle_site_symmetry_3
      _geom_angle_publ_flag
  O9        Al1       O10               110.8(9)      5_555  .      1_555  N
  O9        Al1       O11               105.8(9)      5_555  .      7_455  N
  O9        Al1       O12               121.3(9)      5_555  .      8_555  N
  O10       Al1       O11               106.0(8)      1_555  .      7_455  N
  O10       Al1       O12               106.4(8)      1_555  .      8_555  N
  O11       Al1       O12               105.5(9)      7_455  .      8_555  N
  O13       Al2       O14               111.9(9)      1_555  .      1_555  N
  O13       Al2       O15               109.3(9)      1_555  .      1_555  N
  O13       Al2       O16               109.0(9)      1_555  .      1_555  N
  O14       Al2       O15               111.9(9)      1_555  .      1_555  N
  O14       Al2       O16               109.6(9)      1_555  .      1_555  N
  O15       Al2       O16               104.8(8)      1_555  .      1_555  N
  O18       Al3       O19               110.7(9)      1_555  .      1_555  N
  O18       Al3       O23               110.6(8)      1_555  .      8_555  N
  O18       Al3       O24               107.7(9)      1_555  .      1_555  N
  O19       Al3       O23               112.6(8)      1_555  .      8_555  N
  O19       Al3       O24               109.7(9)      1_555  .      1_555  N
  O23       Al3       O24               105.2(8)      8_555  .      1_555  N
  O17       Al4       O20               107.1(8)      1_555  .      7_455  N
  O17       Al4       O21               110.5(8)      1_555  .      8_555  N
  O17       Al4       O22               113.6(9)      1_555  .      5_555  N
  O20       Al4       O21               107.1(9)      7_455  .      8_555  N
  O20       Al4       O22               105.4(8)      7_455  .      5_555  N
  O21       Al4       O22               112.6(9)      8_555  .      5_555  N
  O10       P5        O13               111.8(9)      1_555  .      1_555  N
  O10       P5        O17               107.0(7)      1_555  .      1_555  N
  O10       P5        O18               112.0(9)      1_555  .      1_555  N
  O13       P5        O17               106.3(9)      1_555  .      1_555  N
  O13       P5        O18               109.0(8)      1_555  .      1_555  N
  O17       P5        O18               110.6(9)      1_555  .      1_555  N
  O9        P6        O11               107.3(9)      1_555  .      1_555  N
  O9        P6        O15               115.7(9)      1_555  .      1_555  N
  O9        P6        O19               111.4(9)      1_555  .      8_554  N
  O11       P6        O15               104.2(8)      1_555  .      1_555  N
  O11       P6        O19              110.4(10)      1_555  .      8_554  N
  O15       P6        O19               107.5(8)      1_555  .      8_554  N
  O16       P7        O20               107.3(9)      1_555  .      1_455  N
  O16       P7        O21               110.0(8)      1_555  .      1_555  N
  O16       P7        O22               110.3(8)      1_555  .      1_555  N
  O20       P7        O21               109.3(9)      1_455  .      1_555  N
  O20       P7        O22               111.5(9)      1_455  .      1_555  N
  O21       P7        O22               108.5(9)      1_555  .      1_555  N
  O12       P8        O14               114.4(9)      1_555  .      1_555  N
  O12       P8        O23               109.2(8)      1_555  .      1_555  N
  O12       P8        O24               104.2(9)      1_555  .      5_555  N
  O14       P8        O23               109.7(9)      1_555  .      1_555  N
  O14       P8        O24               108.8(8)      1_555  .      5_555  N
  O23       P8        O24               110.4(8)      1_555  .      5_555  N
  Al1       O9        P6               143.0(10)      5_545  .      1_555  N
  Al1       O10       P5                136.7(9)      1_555  .      1_555  N
  Al1       O11       P6               135.2(10)      7_555  .      1_555  N
  Al1       O12       P8               174.6(12)      8_554  .      1_555  N
  Al2       O13       P5               161.5(12)      1_555  .      1_555  N
  Al2       O14       P8                145.2(9)      1_555  .      1_555  N
  Al2       O15       P6                165.1(9)      1_555  .      1_555  N
  Al2       O16       P7                130.9(8)      1_555  .      1_555  N
  Al4       O17       P5                143.5(8)      1_555  .      1_555  N
  Al3       O18       P5                160.9(9)      1_555  .      1_555  N
  Al3       O19       P6                143.5(8)      1_555  .      8_555  N
  Al4       O20       P7               171.8(12)      7_555  .      1_655  N
  Al4       O21       P7               132.4(10)      8_554  .      1_555  N
  Al4       O22       P7                134.9(9)      5_545  .      1_555  N
  Al3       O23       P8                137.7(8)      8_554  .      1_555  N
  Al3       O24       P8               137.4(10)      1_555  .      5_545  N

# Powder diffraction data for histogram  1
#==============================================================================
# 9. INSTRUMENT CHARACTERIZATION

_exptl_special_details
; ?
;

# if regions of the data are excluded, the reason(s) are supplied here:
_pd_proc_info_excluded_regions
; ?
;

# The following item is used to identify the equipment used to record
# the powder pattern when the diffractogram was measured at a laboratory
# other than the authors' home institution, e.g. when neutron or synchrotron
# radiation is used.

_pd_instr_location
; ?
;
_pd_calibration_special_details           # description of the method used
                                          # to calibrate the instrument
; ?
;

_diffrn_ambient_temperature       ?
_diffrn_source                    ?
_diffrn_source_target             ?
_diffrn_source_type               ?
_diffrn_measurement_device_type   ?
_diffrn_detector                  ?
_diffrn_detector_type             ?       # make or model of detector

_pd_meas_scan_method              ?       # options are 'step', 'cont',
                                          # 'tof', 'fixed' or
                                          # 'disp' (= dispersive)
_pd_meas_special_details
;  ?
;

# The following two items identify the program(s) used (if appropriate).
_computing_data_collection        ?
_computing_data_reduction         ?

# Describe any processing performed on the data, prior to refinement.
# For example: a manual Lp correction or a precomputed absorption correction
_pd_proc_info_data_reduction      ?

# The following item is used for angular dispersive measurements only.

_diffrn_radiation_monochromator   ?

# The following items are used to define the size of the instrument.
# Not all distances are appropriate for all instrument types.

_pd_instr_dist_src/mono           ?
_pd_instr_dist_mono/spec          ?
_pd_instr_dist_src/spec           ?
_pd_instr_dist_spec/anal          ?
_pd_instr_dist_anal/detc          ?
_pd_instr_dist_spec/detc          ?

# 10. Specimen size and mounting information

# The next three fields give the specimen dimensions in mm.  The equatorial
# plane contains the incident and diffracted beam.

_pd_spec_size_axial               ?       # perpendicular to
                                          # equatorial plane

_pd_spec_size_equat               ?       # parallel to
                                          # scattering vector
                                          # in transmission

_pd_spec_size_thick               ?       # parallel to
                                          # scattering vector
                                          # in reflection

_pd_spec_mounting                         # This field should be
                                          # used to give details of the
                                          # container.
; ?
;

_pd_spec_mount_mode               ?       # options are 'reflection'
                                          # or 'transmission'

_pd_spec_shape                    ?       # options are 'cylinder'
                                          # 'flat_sheet' or 'irregular'


loop_ _atom_type_symbol
      _atom_type_number_in_cell
      _atom_type_scat_dispersion_real
      _atom_type_scat_dispersion_imag
      _atom_type_scat_Cromer_Mann_a1
      _atom_type_scat_Cromer_Mann_a2
      _atom_type_scat_Cromer_Mann_a3
      _atom_type_scat_Cromer_Mann_a4
      _atom_type_scat_Cromer_Mann_b1
      _atom_type_scat_Cromer_Mann_b2
      _atom_type_scat_Cromer_Mann_b3
      _atom_type_scat_Cromer_Mann_b4
      _atom_type_scat_Cromer_Mann_c
      _atom_type_scat_source
  Al        32.0    0.000    0.000
 6.42020 3.03870 1.90020 0.74260 1.59360 31.5472 1.96460 85.0886 1.11510 
  International_Tables_Vol_C
  P         32.0    0.000    0.000
 6.43450 1.90670 4.17910 27.1570 1.78000 0.52600 1.49080 68.1645 1.11490 
  International_Tables_Vol_C
  O         128.0    0.000    0.000
 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 
  International_Tables_Vol_C
_diffrn_radiation_probe                x-ray
_diffrn_radiation_polarisn_ratio       ?
_diffrn_radiation_wavelength           0.692648
_diffrn_radiation_type                 ?
_pd_proc_ls_prof_R_factor              0.0512
_pd_proc_ls_prof_wR_factor             0.0690
_pd_proc_ls_prof_wR_expected           0.0207
_refine_ls_R_Fsqd_factor               0.08700

_pd_proc_ls_background_function
;   GSAS Background function number 1 with 26 terms.
 Shifted Chebyshev function of 1st kind
      1:    1641.76     2:   -672.060     3:    116.383     4:    105.862    
      5:   -243.739     6:    97.5744     7:    175.944     8:   -156.124    
      9:    22.4820    10:    34.0399    11:   -85.8467    12:    8.55213    
     13:    40.5670    14:   -40.2147    15:   -3.56798    16:    24.7632    
     17:   -19.9129    18:   -1.13889    19:   -20.8363    20:    27.0855    
     21:    1.68008    22:   -20.8287    23:    42.2233    24:   -15.7005    
     25:   -17.2717    26:    23.1672    
;

_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_absorpt_correction_T_min        1.00000
_exptl_absorpt_correction_T_max        1.00000
# Extinction correction
_gsas_exptl_extinct_corr_T_min         1.00000
_gsas_exptl_extinct_corr_T_max         1.00000

_pd_proc_ls_profile_function
;
 CW Profile function number 4 with  16 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 Microstrain broadening by P.W. Stephens,  (1999). J. Appl. Cryst.,32,281-289.
 #1(GU)   =    0.000 #2(GV)   =   35.455 #3(GW)   =    1.840
 #4(GP)   =    1.064 #5(LX)   =    0.000 #6(ptec) =     1.32
 #7(trns) =     0.00 #8(shft) =   0.0000 #9(sfec) =     0.00
 #10(S/L) =   0.0145 #11(H/L) =   0.0044 #12(eta) =   0.9896
 #13(S400 ) =  2.0E-02 #14(S004 ) =  3.5E-02
 #15(S220 ) =  3.7E-02 #16(S202 ) =  1.1E-01
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_peak_cutoff 0.00100
_pd_proc_info_datetime                 2018-07-25T12:51:20
_pd_calc_method                        "Rietveld Refinement"

#---- raw/calc data loop -----
_pd_meas_2theta_range_min              0.0077
_pd_meas_2theta_range_max              49.1027
_pd_meas_2theta_range_inc              0.015
_pd_proc_2theta_range_min              -0.02692
_pd_proc_2theta_range_max              49.06808
_pd_proc_2theta_range_inc              0.015

loop_
      _pd_meas_counts_total
      _pd_proc_ls_weight
      _pd_proc_intensity_bkg_calc
      _pd_calc_intensity_total
   0.0       0.0        -10504891.00000   .
   0.0       0.0        -10137111.00000   .
   0.0       0.0        -9781181.00000    .
   0.0       0.0        -9436756.00000    .
   0.0       0.0        -9103494.00000    .
   0.0       0.0        -8781054.00000    .
   0.0       0.0        -8469127.00000    .
   0.0       0.0        -8167388.50000    .
   0.0       0.0        -7875536.50000    .
   0.0       0.0        -7593275.00000    .
   0.0       0.0        -7320313.00000    .
   0.0       0.0        -7056371.50000    .
   0.0       0.0        -6801175.00000    .
   0.0       0.0        -6554455.00000    .
   0.0       0.0        -6315960.00000    .
   0.0       0.0        -6085434.50000    .
   0.0       0.0        -5862634.50000    .
   0.0       0.0        -5647327.00000    .
   0.0       0.0        -5439276.50000    .
   0.0       0.0        -5238259.50000    .
   0.0       0.0        -5044058.50000    .
   0.0       0.0        -4856463.50000    .
   0.0       0.0        -4675270.00000    .
   0.0       0.0        -4500274.00000    .
   0.0       0.0        -4331285.50000    .
   0.0       0.0        -4168112.00000    .
   0.0       0.0        -4010575.00000    .
   0.0       0.0        -3858492.25000    .
   0.0       0.0        -3711692.50000    .
   0.0       0.0        -3570008.50000    .
   0.0       0.0        -3433280.50000    .
   0.0       0.0        -3301342.00000    .
   0.0       0.0        -3174046.00000    .
   0.0       0.0        -3051243.25000    .
   0.0       0.0        -2932786.00000    .
   0.0       0.0        -2818537.25000    .
   0.0       0.0        -2708356.75000    .
   0.0       0.0        -2602115.25000    .
   0.0       0.0        -2499682.50000    .
   0.0       0.0        -2400935.75000    .
   0.0       0.0        -2305752.25000    .
   0.0       0.0        -2214016.50000    .
   0.0       0.0        -2125613.25000    .
   0.0       0.0        -2040431.37500    .
   0.0       0.0        -1958366.62500    .
   0.0       0.0        -1879313.37500    .
   0.0       0.0        -1803171.50000    .
   0.0       0.0        -1729841.87500    .
   0.0       0.0        -1659232.62500    .
  26.0       0.0        -1591248.75000    .
  31.0       0.0        -1525805.25000    .
  36.0       0.0        -1462813.75000    .
  47.0       0.0        -1402189.87500    .
  61.0       0.0        -1343853.50000    .
  75.0       0.0        -1287725.75000    .
  88.0       0.0        -1233731.50000    .
  101.0      0.0        -1181796.37500    .
  113.0      0.0        -1131850.00000    .
  126.0      0.0        -1083822.25000    .
  137.0      0.0        -1037646.43750    .
  148.0      0.0        -993257.31250     .
  160.0      0.0        -950594.12500     .
  175.0      0.0        -909593.62500     .
  191.0      0.0        -870198.18750     .
  208.0      0.0        -832350.37500     .
  227.0      0.0        -795995.87500     .
  254.0      0.0        -761080.12500     .
  290.0      0.0        -727552.68750     .
  330.0      0.0        -695363.12500     .
  376.0      0.0        -664463.00000     .
  423.0      0.0        -634805.81250     .
  466.0      0.0        -606346.18750     .
  504.0      0.0        -579040.12500     .
  536.0      0.0        -552845.81250     .
  568.0      0.0        -527721.75000     .
  600.0      0.0        -503629.06250     .
  632.0      0.0        -480529.31250     .
  661.0      0.0        -458385.28125     .
  693.0      0.0        -437161.81250     .
  724.0      0.0        -416823.37500     .
  754.0      0.0        -397337.87500     .
  785.0      0.0        -378672.37500     .
  816.0      0.0        -360795.75000     .
  846.0      0.0        -343677.81250     .
  871.0      0.0        -327290.15625     .
  899.0      0.0        -311604.31250     .
  923.0      0.0        -296593.25000     .
  943.0      0.0        -282230.62500     .
  963.0      0.0        -268491.71875     .
  984.0      0.0        -255351.73438     .
  1008.0     0.0        -242787.35938     .
  1030.0     0.0        -230775.96875     .
  1050.0     0.0        -219295.67188     .
  1073.0     0.0        -208325.50000     .
  1099.0     0.0        -197844.68750     .
  1122.0     0.0        -187834.12500     .
  1141.0     0.0        -178274.70313     .
  1155.0     0.0        -169148.10938     .
  1165.0     0.0        -160436.76563     .
  1173.0     0.0        -152123.79688     .
  1178.0     0.0        -144193.01563     .
  1183.0     0.0        -136628.42188     .
  1188.0     0.0        -129415.03125     .
  1194.0     0.0        -122538.39844     .
  1200.0     0.0        -115984.18750     .
  1208.0     0.0        -109738.98438     .
  1219.0     0.0        -103789.92969     .
  1236.0     0.0        -98124.25781      .
  1268.0     0.0        -92729.98438      .
  1324.0     0.0        -87595.57813      .
  1412.0     0.0        -82709.77344      .
  1534.0     0.0        -78062.00000      .
  1692.0     0.0        -73641.76563      .
  1885.0     0.0        -69439.17969      .
  2090.0     0.0        -65444.72656      .
  2276.0     0.0        -61649.26563      .
  2420.0     0.0        -58043.83203      .
  2513.0     0.0        -54620.19531      .
  2557.0     0.0        -51370.05469      .
  2570.0     0.0        -48285.67188      .
  2562.0     0.0        -45359.48438      .
  2543.0     0.0        -42584.33203      .
  2525.0     0.0        -39953.30859      .
  2505.0     0.0        -37459.76563      .
  2482.0     0.0        -35097.33203      .
  2464.0     0.0        -32859.91016      .
  2448.0     0.0        -30741.69141      .
  2432.0     0.0        -28737.00977      .
  2414.0     0.0        -26840.50977      .
  2400.0     0.0        -25047.01563      .
  2383.0     0.0        -23351.61133      .
  2369.0     0.0        -21749.55078      .
  2355.0     0.0        -20236.34180      .
  2340.0     0.0        -18807.56445      .
  2326.0     0.0        -17459.17578      .
  2316.0     0.0        -16187.10156      .
  2308.0     0.0        -14987.62500      .
  2292.0     0.0        -13857.03223      .
  2274.0     0.0        -12791.89941      .
  2259.0     0.0        -11788.89453      .
  2249.0     0.0        -10844.82910      .
  2240.0     0.0        -9956.68359       .
  2235.0     0.0        -9121.52930       .
  2231.0     0.0        -8336.65137       .
  2226.0     0.0        -7599.35352       .
  2216.0     0.0        -6907.15186       .
  2205.0     0.0        -6257.63135       .
  2197.0     0.0        -5648.47949       .
  2189.0     0.0        -5077.54639       .
  2181.0     0.0        -4542.71826       .
  2177.0     0.0        -4042.01392       .
  2171.0     0.0        -3573.55078       .
  2163.0     0.0        -3135.52954       .
  2158.0     0.0        -2726.21899       .
  2155.0     0.0        -2344.00146       .
  2151.0     0.0        -1987.32935       .
  2144.0     0.0        -1654.72180       .
  2132.0     0.0        -1344.77930       .
  2121.0     0.0        -1056.16528       .
  2116.0     0.0        -787.62512        .
  2115.0     0.0        -537.94995        .
  2122.0     0.0        -306.00629        .
  2133.0     0.0        -90.71359         .
  2141.0     0.0         108.95684        .
  2151.0     0.0         293.96429        .
  2165.0     0.0         465.23911        .
  2179.0     0.0         623.64380        .
  2190.0     0.0         770.00574        .
  2196.0     0.0         905.09937        .
  2196.0     0.0         1029.66431       .
  2192.0     0.0         1144.39307       .
  2182.0     0.0         1249.93958       .
  2166.0     0.0         1346.92908       .
  2146.0     0.0         1435.94360       .
  2127.0     0.0         1517.53052       .
  2114.0     0.0         1592.21289       .
  2108.0     0.0         1660.47632       .
  2105.0     0.0         1722.78125       .
  2103.0     0.0         1779.55908       .
  2105.0     0.0         1831.21704       .
  2110.0     0.0         1878.13428       .
  2123.0     0.0         1920.66943       .
  2151.0     0.0         1959.15710       .
  2195.0     0.0         1993.91077       .
  2253.0     0.0         2025.22571       .
  2316.0     0.0         2053.37451       .
  2367.0     0.0         2078.61572       .
  2392.0     0.0         2101.18750       .
  2390.0     0.0         2121.31396       .
  2377.0     0.0         2139.20337       .
  2360.0     0.0         2155.04858       .
  2346.0     0.0         2169.03101       .
  2338.0     0.0         2181.31592       .
  2334.0     0.0         2192.05981       .
  2332.0     0.0         2201.40576       .
  2332.0     0.0         2209.48657       .
  2333.0     0.0         2216.42505       .
  2334.0     0.0         2222.33423       .
  2331.0     0.0         2227.31836       .
  2321.0     0.0         2231.47339       .
  2306.0     0.000434    2234.88721       2253.97827
  2289.0     0.000437    2237.64063       2257.84180
  2274.0     0.000440    2239.80664       2261.21997
  2266.0     0.000441    2241.45313       2264.19287
  2263.0     0.000442    2242.64111       2266.83667
  2262.0     0.000442    2243.42603       2269.22437
  2259.0     0.000443    2243.85864       2271.42700
  2258.0     0.000443    2243.98364       2273.51440
  2259.0     0.000443    2243.84277       2275.55591
  2260.0     0.000442    2243.47241       2277.62305
  2264.0     0.000442    2242.90552       2279.79053
  2269.0     0.000441    2242.17114       2282.13818
  2277.0     0.000439    2241.29541       2284.75366
  2288.0     0.000437    2240.30151       2287.73706
  2304.0     0.000434    2239.20898       2291.20410
  2319.0     0.000431    2238.03564       2295.57739
  2331.0     0.000429    2236.79639       2300.47437
  2344.0     0.000427    2235.50439       2306.38159
  2357.0     0.000424    2234.17041       2313.57935
  2372.0     0.000422    2232.80420       2322.43823
  2395.0     0.000418    2231.41284       2356.40625
  2422.0     0.000413    2230.00269       2370.97021
  2455.0     0.000407    2228.57837       2389.65552
  2492.0     0.000401    2227.14404       2414.72485
  2539.0     0.000394    2225.70190       2450.98462
  2596.0     0.000385    2224.25391       2508.15576
  2664.0     0.000375    2222.80078       2602.87646
  2748.0     0.000364    2221.34302       2757.85205
  2859.0     0.0003498   2219.88013       2993.70508
  3007.0     0.0003326   2218.41113       3320.63672
  3211.0     0.0003114   2216.93481       3756.18555
  3504.0     0.0002854   2215.44946       4296.57861
  3945.0     0.0002535   2213.95313       4963.63672
  4621.0     0.0002164   2212.44360       5771.16992
  5633.0     0.0001775   2210.91870       6733.65869
  7005.0     0.0001428   2209.37598       7800.80420
  8529.0     0.0001172   2207.81299       8801.71484
  9702.0     0.0001031   2206.22705       9359.46875
  9864.0     0.0001014   2204.61572       8982.94434
  8773.0     0.0001140   2202.97681       7509.49609
  6987.0     0.0001431   2201.30786       5662.42725
  5285.0     0.0001892   2199.60669       4216.78076
  4151.0     0.0002409   2197.87134       3348.73926
  3538.0     0.0002826   2196.09985       2907.78076
  3189.0     0.0003136   2194.29077       2695.52661
  2974.0     0.0003362   2192.44238       2583.56885
  2824.0     0.000354    2190.55371       2514.16797
  2716.0     0.000368    2188.62354       2465.86792
  2635.0     0.000380    2186.65112       2430.37109
  2570.0     0.000389    2184.63599       2403.65112
  2521.0     0.000397    2182.57764       2383.40503
  2478.0     0.000404    2180.47632       2368.45972
  2440.0     0.000410    2178.33228       2358.83813
  2413.0     0.000414    2176.14575       2355.85840
  2396.0     0.000417    2173.91772       2361.48926
  2385.0     0.000419    2171.64893       2376.94531
  2378.0     0.000421    2169.34058       2402.36157
  2377.0     0.000421    2166.99414       2438.13452
  2383.0     0.000420    2164.61157       2486.00684
  2402.0     0.000416    2162.19434       2548.95239
  2435.0     0.000411    2159.74487       2629.35034
  2471.0     0.000405    2157.26514       2721.68359
  2497.0     0.000400    2154.75806       2796.92847
  2495.0     0.000401    2152.22607       2798.47900
  2465.0     0.000406    2149.67188       2690.91260
  2426.0     0.000412    2147.09888       2536.87573
  2397.0     0.000417    2144.51001       2424.87207
  2387.0     0.000419    2141.90894       2374.48364
  2386.0     0.000419    2139.29858       2362.22974
  2390.0     0.000418    2136.68262       2365.37427
  2396.0     0.000417    2134.06519       2374.30981
  2403.0     0.000416    2131.44946       2386.66406
  2414.0     0.000414    2128.83960       2402.17725
  2428.0     0.000412    2126.23975       2427.93506
  2446.0     0.000409    2123.65332       2450.92822
  2472.0     0.000405    2121.08472       2478.49365
  2505.0     0.000399    2118.53784       2511.55420
  2543.0     0.000393    2116.01709       2551.34448
  2588.0     0.000386    2113.52588       2599.51782
  2645.0     0.000378    2111.06909       2658.32178
  2719.0     0.000368    2108.65039       2730.86938
  2817.0     0.000355    2106.27368       2821.64404
  2950.0     0.0003390   2103.94336       2937.63135
  3140.0     0.0003185   2101.66333       3091.30127
  3416.0     0.0002927   2099.43750       3307.79468
  3831.0     0.0002610   2097.26978       3638.23877
  4475.0     0.0002235   2095.16406       4176.13916
  5486.0     0.0001823   2093.12402       5067.06055
  7044.0     0.0001420   2091.15308       6493.72852
  9363.0     0.0001068   2089.25537       8608.61230
  12637.0    0.0000791   2087.43384       11546.60254
  16983.0    0.0000589   2085.69214       15486.93945
  22201.0    0.0000450   2084.03369       20374.18750
  28036.0    0.0000357   2082.46118       26140.08008
  33578.0    0.0000298   2080.97803       31965.30078
  36855.0    0.0000271   2079.58716       36289.97656
  35869.0    0.0000279   2078.29102       36742.70703
  30239.0    0.0000331   2077.09229       31734.13281
  21828.0    0.0000458   2075.99390       23204.05273
  14044.0    0.0000712   2074.99756       15230.43164
  8783.0     0.0001139   2074.10571       9741.67090
  5806.0     0.0001722   2073.32056       6609.43750
  4293.0     0.0002329   2072.64404       5004.47559
  3533.0     0.0002830   2072.07739       4179.74512
  3128.0     0.0003197   2071.62256       3705.26416
  2892.0     0.0003458   2071.28101       3392.07861
  2739.0     0.000365    2071.05371       3166.05811
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  4107.0     0.0002435   1912.71057       3775.76611
  4045.0     0.0002472   1906.87988       3622.05103
  3925.0     0.0002548   1901.02380       3445.10376
  3698.0     0.0002704   1895.14355       3279.53735
  3395.0     0.0002946   1889.23999       3150.64307
  3105.0     0.0003221   1883.31323       3061.42871
  2906.0     0.0003441   1877.36401       2991.99414
  2790.0     0.000358    1871.39368       2909.81445
  2694.0     0.000371    1865.40198       2798.09692
  2571.0     0.000389    1859.39014       2671.45996
  2423.0     0.000413    1853.35901       2553.81616
  2283.0     0.000438    1847.30872       2457.83911
  2182.0     0.000458    1841.24084       2384.56323
  2130.0     0.000469    1835.15503       2329.62354
  2109.0     0.000474    1829.05273       2288.63110
  2099.0     0.000476    1822.93494       2258.93457
  2083.0     0.000480    1816.80151       2237.16431
  2054.0     0.000487    1810.65369       2218.10962
  2018.0     0.000496    1804.49292       2195.73364
  1985.0     0.000504    1798.31873       2167.59204
  1959.0     0.000510    1792.13257       2136.69214
  1943.0     0.000515    1785.93567       2108.30542
  1941.0     0.000515    1779.72778       2085.92725
  1951.0     0.000513    1773.51074       2071.43530
  1968.0     0.000508    1767.28442       2058.63477
  1979.0     0.000505    1761.05017       2044.28455
  1974.0     0.000507    1754.80908       2028.21021
  1950.0     0.000513    1748.56128       2013.39441
  1918.0     0.000521    1742.30786       2002.16187
  1895.0     0.000528    1736.05017       1994.20508
  1889.0     0.000529    1729.78821       1987.36121
  1896.0     0.000527    1723.52319       1979.61548
  1907.0     0.000524    1717.25647       1971.26501
  1913.0     0.000523    1710.98816       1964.35901
  1913.0     0.000523    1704.71924       1962.81116
  1912.0     0.000523    1698.45105       1971.49377
  1927.0     0.000519    1692.18372       1995.74695
  1969.0     0.000508    1685.91895       2051.36035
  2051.0     0.000488    1679.65686       2152.38916
  2187.0     0.000457    1673.39832       2316.06689
  2391.0     0.000418    1667.14514       2551.93945
  2664.0     0.000375    1660.89697       2849.76074
  2982.0     0.0003353   1654.65527       3160.75708
  3273.0     0.0003055   1648.42126       3380.42725
  3434.0     0.0002912   1642.19507       3394.24243
  3396.0     0.0002945   1635.97791       3207.27612
  3186.0     0.0003139   1629.77100       2939.69800
  2921.0     0.0003423   1623.57446       2696.85498
  2723.0     0.000367    1617.39001       2527.15723
  2649.0     0.000378    1611.21765       2438.88892
  2668.0     0.000375    1605.05859       2416.13623
  2739.0     0.000365    1598.91418       2428.20459
  2819.0     0.000355    1592.78442       2439.32764
  2862.0     0.0003494   1586.67078       2421.94434
  2825.0     0.000354    1580.57410       2370.89185
  2692.0     0.000371    1574.49475       2301.74438
  2497.0     0.000400    1568.43396       2235.13306
  2300.0     0.000435    1562.39270       2185.57446
  2151.0     0.000465    1556.37146       2160.06714
  2067.0     0.000484    1550.37122       2159.98486
  2033.0     0.000492    1544.39307       2181.95459
  2030.0     0.000493    1538.43738       2217.76123
  2045.0     0.000489    1532.50537       2253.51953
  2073.0     0.000482    1526.59753       2275.50513
  2114.0     0.000473    1520.71472       2272.89160
  2158.0     0.000463    1514.85828       2241.66064
  2187.0     0.000457    1509.02820       2188.31494
  2182.0     0.000458    1503.22559       2128.23193
  2135.0     0.000468    1497.45178       2078.28711
  2062.0     0.000485    1491.70667       2051.90063
  1996.0     0.000501    1485.99146       2058.68262
  1968.0     0.000508    1480.30737       2104.77637
  1992.0     0.000502    1474.65430       2192.08105
  2068.0     0.000484    1469.03381       2315.17261
  2181.0     0.000459    1463.44580       2455.16113
  2306.0     0.000434    1457.89160       2573.58838
  2410.0     0.000415    1452.37207       2626.45679
  2470.0     0.000405    1446.88745       2607.22827
  2487.0     0.000402    1441.43860       2560.20020
  2504.0     0.000399    1436.02661       2537.45215
  2564.0     0.000390    1430.65161       2568.49854
  2675.0     0.000374    1425.31458       2655.27612
  2792.0     0.000358    1420.01648       2763.20410
  2838.0     0.000352    1414.75745       2815.52148
  2754.0     0.000363    1409.53833       2737.71143
  2542.0     0.000393    1404.36011       2541.74268
  2270.0     0.000441    1399.22290       2303.76074
  2019.0     0.000495    1394.12781       2084.69409
  1833.0     0.000546    1389.07495       1912.13599
  1717.0     0.000582    1384.06519       1791.30969
  1648.0     0.000607    1379.09949       1715.39978
  1608.0     0.000622    1374.17786       1674.06506
  1585.0     0.000631    1369.30103       1655.43982
  1577.0     0.000634    1364.46985       1652.99805
  1583.0     0.000632    1359.68457       1661.63928
  1605.0     0.000623    1354.94580       1676.59192
  1644.0     0.000608    1350.25439       1691.85510
  1698.0     0.000589    1345.61023       1699.62305
  1757.0     0.000569    1341.01453       1692.46436
  1799.0     0.000556    1336.46692       1668.42285
  1802.0     0.000555    1331.96887       1632.00317
  1760.0     0.000568    1327.52039       1591.47913
  1686.0     0.000593    1323.12134       1550.80554
  1606.0     0.000623    1318.77332       1514.12866
  1541.0     0.000649    1314.47632       1482.62195
  1496.0     0.000668    1310.23059       1454.61646
  1467.0     0.000682    1306.03601       1433.13367
  1448.0     0.000691    1301.89417       1415.73755
  1434.0     0.000697    1297.80481       1401.73132
  1425.0     0.000702    1293.76770       1390.69336
  1419.0     0.000705    1289.78442       1381.72217
  1417.0     0.000706    1285.85474       1373.08020
  1416.0     0.000706    1281.97839       1367.79529
  1417.0     0.000706    1278.15686       1364.06018
  1420.0     0.000704    1274.38977       1361.91870
  1425.0     0.000702    1270.67712       1361.46802
  1428.0     0.000700    1267.01990       1362.98767
  1428.0     0.000700    1263.41809       1367.24365
  1425.0     0.000702    1259.87146       1375.70264
  1423.0     0.000703    1256.38110       1390.47070
  1424.0     0.000702    1252.94666       1412.87854
  1430.0     0.000699    1249.56824       1444.35571
  1443.0     0.000693    1246.24658       1484.54810
  1461.0     0.000684    1242.98157       1529.34863
  1483.0     0.000674    1239.77295       1570.44861
  1503.0     0.000665    1236.62170       1596.55847
  1516.0     0.000660    1233.52759       1601.19763
  1520.0     0.000658    1230.49011       1588.03979
  1515.0     0.000660    1227.51050       1568.37610
  1510.0     0.000662    1224.58826       1555.40894
  1508.0     0.000663    1221.72351       1555.04993
  1518.0     0.000659    1218.91602       1568.46545
  1543.0     0.000648    1216.16638       1591.52039
  1586.0     0.000631    1213.47449       1615.00757
  1644.0     0.000608    1210.83984       1626.75635
  1697.0     0.000589    1208.26343       1617.94067
  1722.0     0.000581    1205.74451       1589.40967
  1704.0     0.000587    1203.28296       1550.38477
  1648.0     0.000607    1200.87952       1510.94067
  1575.0     0.000635    1198.53357       1478.60730
  1509.0     0.000663    1196.24487       1458.28101
  1464.0     0.000683    1194.01404       1454.19189
  1438.0     0.000695    1191.84058       1472.45850
  1430.0     0.000699    1189.72412       1518.14001
  1434.0     0.000697    1187.66516       1594.60461
  1444.0     0.000693    1185.66321       1696.66992
  1456.0     0.000687    1183.71802       1804.95789
  1466.0     0.000682    1181.82983       1880.88733
  1471.0     0.000680    1179.99841       1880.10205
  1473.0     0.000679    1178.22302       1798.82581
  1475.0     0.000678    1176.50427       1679.78564
  1478.0     0.000677    1174.84155       1563.48706
  1481.0     0.000675    1173.23438       1471.12756
  1482.0     0.000675    1171.68323       1408.94006
  1480.0     0.000676    1170.18738       1372.84985
  1476.0     0.000678    1168.74658       1354.99158
  1469.0     0.000681    1167.36060       1346.16284
  1455.0     0.000687    1166.02942       1338.17273
  1433.0     0.000698    1164.75256       1323.59131
  1405.0     0.000712    1163.52954       1303.08228
  1376.0     0.000727    1162.36035       1281.23962
  1353.0     0.000739    1161.24463       1261.86133
  1339.0     0.000747    1160.18176       1246.53760
  1330.0     0.000752    1159.17188       1234.52600
  1324.0     0.000755    1158.21436       1227.14258
  1321.0     0.000757    1157.30872       1222.25891
  1321.0     0.000757    1156.45471       1219.54089
  1325.0     0.000755    1155.65210       1218.79968
  1335.0     0.000749    1154.90015       1219.86475
  1352.0     0.000740    1154.19873       1222.84058
  1377.0     0.000726    1153.54736       1227.53394
  1407.0     0.000711    1152.94556       1233.20593
  1436.0     0.000696    1152.39282       1238.21155
  1452.0     0.000689    1151.88904       1240.32593
  1448.0     0.000691    1151.43323       1238.78320
  1426.0     0.000701    1151.02539       1235.32349
  1395.0     0.000717    1150.66479       1232.17834
  1367.0     0.000732    1150.35107       1230.71204
  1351.0     0.000740    1150.08374       1231.54321
  1344.0     0.000744    1149.86218       1235.18164
  1344.0     0.000744    1149.68591       1241.22766
  1349.0     0.000741    1149.55457       1250.08960
  1357.0     0.000737    1149.46741       1262.03113
  1367.0     0.000732    1149.42395       1277.51318
  1378.0     0.000726    1149.42383       1296.95483
  1391.0     0.000719    1149.46631       1320.58691
  1405.0     0.000712    1149.55078       1348.29089
  1419.0     0.000705    1149.67688       1379.35315
  1438.0     0.000695    1149.84399       1412.88672
  1461.0     0.000684    1150.05139       1447.01990
  1491.0     0.000671    1150.29871       1477.90344
  1530.0     0.000654    1150.58521       1500.40808
  1571.0     0.000637    1150.91016       1511.18262
  1602.0     0.000624    1151.27332       1510.47974
  1613.0     0.000620    1151.67371       1503.39368
  1604.0     0.000623    1152.11096       1495.89075
  1584.0     0.000631    1152.58447       1492.64111
  1567.0     0.000638    1153.09338       1496.94019
  1564.0     0.000639    1153.63721       1511.04919
  1580.0     0.000633    1154.21545       1535.35400
  1610.0     0.000621    1154.82727       1566.69165
  1640.0     0.000610    1155.47205       1597.00110
  1651.0     0.000606    1156.14917       1618.14709
  1633.0     0.000612    1156.85803       1630.39099
  1592.0     0.000628    1157.59790       1642.48352
  1544.0     0.000648    1158.36804       1661.98462
  1510.0     0.000662    1159.16821       1689.83289
  1494.0     0.000669    1159.99719       1720.21692
  1491.0     0.000671    1160.85461       1741.50903
  1494.0     0.000669    1161.73975       1742.75769
  1497.0     0.000668    1162.65198       1726.25879
  1500.0     0.000667    1163.59045       1706.16333
  1504.0     0.000665    1164.55481       1696.61401
  1513.0     0.000661    1165.54407       1709.80188
  1528.0     0.000654    1166.55762       1751.44324
  1550.0     0.000645    1167.59509       1822.14441
  1585.0     0.000631    1168.65527       1915.27844
  1634.0     0.000612    1169.73767       2014.60706
  1698.0     0.000589    1170.84204       2097.69849
  1782.0     0.000561    1171.96704       2150.25610
  1893.0     0.000528    1173.11230       2171.83447
  2022.0     0.000495    1174.27722       2162.27319
  2131.0     0.000469    1175.46094       2120.42896
  2169.0     0.000461    1176.66272       2052.78564
  2117.0     0.000472    1177.88220       1973.90930
  1998.0     0.000501    1179.11829       1900.94824
  1866.0     0.000536    1180.37061       1847.18567
  1769.0     0.000565    1181.63843       1821.09827
  1729.0     0.000578    1182.92090       1825.98962
  1740.0     0.000575    1184.21753       1863.88416
  1790.0     0.000559    1185.52747       1927.46643
  1865.0     0.000536    1186.85034       2000.54480
  1940.0     0.000515    1188.18506       2055.44727
  1987.0     0.000503    1189.53113       2066.32788
  1991.0     0.000502    1190.88831       2031.09851
  1950.0     0.000513    1192.25513       1968.87817
  1881.0     0.000532    1193.63135       1897.52246
  1801.0     0.000555    1195.01660       1827.55652
  1727.0     0.000579    1196.40967       1765.95532
  1669.0     0.000599    1197.81018       1717.47424
  1636.0     0.000611    1199.21765       1684.17627
  1628.0     0.000614    1200.63098       1666.31958
  1640.0     0.000610    1202.04993       1663.55481
  1663.0     0.000601    1203.47375       1674.22620
  1682.0     0.000595    1204.90173       1693.18408
  1686.0     0.000593    1206.33313       1710.46838
  1670.0     0.000599    1207.76782       1715.41223
  1634.0     0.000612    1209.20459       1704.64319
  1590.0     0.000629    1210.64307       1681.40076
  1546.0     0.000647    1212.08276       1650.03162
  1509.0     0.000663    1213.52283       1613.29187
  1483.0     0.000674    1214.96277       1573.68933
  1466.0     0.000682    1216.40222       1534.22925
  1453.0     0.000688    1217.84009       1498.09851
  1444.0     0.000693    1219.27625       1467.74854
  1439.0     0.000695    1220.70984       1444.39783
  1438.0     0.000695    1222.14063       1428.07043
  1446.0     0.000692    1223.56775       1417.96228
  1456.0     0.000687    1224.99060       1412.38989
  1467.0     0.000682    1226.40894       1408.77625
  1472.0     0.000679    1227.82190       1404.30103
  1470.0     0.000680    1229.22900       1397.94629
  1464.0     0.000683    1230.63000       1391.10095
  1460.0     0.000685    1232.02405       1385.90479
  1463.0     0.000684    1233.41064       1383.72888
  1478.0     0.000677    1234.78955       1384.96252
  1507.0     0.000664    1236.15991       1389.17749
  1552.0     0.000644    1237.52148       1395.43445
  1604.0     0.000623    1238.87378       1402.64087
  1649.0     0.000606    1240.21619       1410.20276
  1671.0     0.000598    1241.54810       1418.42725
  1657.0     0.000604    1242.86951       1428.10913
  1614.0     0.000620    1244.17957       1439.72144
  1558.0     0.000642    1245.47791       1452.52966
  1507.0     0.000664    1246.76428       1464.21899
  1474.0     0.000678    1248.03796       1471.67749
  1459.0     0.000685    1249.29858       1471.40552
  1459.0     0.000685    1250.54614       1465.02588
  1463.0     0.000684    1251.77954       1454.80652
  1464.0     0.000683    1252.99890       1443.86462
  1457.0     0.000686    1254.20361       1433.93591
  1441.0     0.000694    1255.39343       1425.83643
  1422.0     0.000703    1256.56775       1421.12793
  1406.0     0.000711    1257.72644       1422.45996
  1401.0     0.000714    1258.86926       1431.25073
  1409.0     0.000710    1259.99548       1448.88403
  1431.0     0.000699    1261.10486       1475.22913
  1464.0     0.000683    1262.19739       1508.69482
  1504.0     0.000665    1263.27246       1545.03833
  1538.0     0.000650    1264.32971       1576.23975
  1556.0     0.000643    1265.36914       1592.48828
  1550.0     0.000645    1266.39014       1588.00928
  1521.0     0.000657    1267.39258       1565.78552
  1477.0     0.000677    1268.37622       1534.71533
  1431.0     0.000699    1269.34070       1503.09827
  1395.0     0.000717    1270.28577       1475.18848
  1371.0     0.000729    1271.21143       1452.11609
  1358.0     0.000736    1272.11707       1433.41370
  1352.0     0.000740    1273.00269       1418.56982
  1354.0     0.000739    1273.86804       1407.60999
  1363.0     0.000734    1274.71277       1400.46338
  1377.0     0.000726    1275.53699       1397.00635
  1394.0     0.000717    1276.34021       1396.58838
  1411.0     0.000709    1277.12231       1398.20447
  1421.0     0.000704    1277.88318       1400.70349
  1427.0     0.000701    1278.62280       1403.47754
  1429.0     0.000700    1279.34082       1407.00452
  1435.0     0.000697    1280.03711       1412.62854
  1447.0     0.000691    1280.71155       1421.09619
  1469.0     0.000681    1281.36414       1433.23096
  1499.0     0.000667    1281.99463       1448.91028
  1532.0     0.000653    1282.60291       1468.21484
  1568.0     0.000638    1283.18909       1491.21399
  1602.0     0.000624    1283.75281       1517.21423
  1629.0     0.000614    1284.29407       1543.58960
  1638.0     0.000611    1284.81299       1564.11987
  1624.0     0.000616    1285.30920       1572.90979
  1592.0     0.000628    1285.78284       1571.04565
  1555.0     0.000643    1286.23401       1564.61340
  1525.0     0.000656    1286.66235       1559.45959
  1509.0     0.000663    1287.06799       1558.25183
  1506.0     0.000664    1287.45105       1560.45068
  1509.0     0.000663    1287.81140       1563.30090
  1517.0     0.000659    1288.14893       1564.36829
  1527.0     0.000655    1288.46387       1560.98779
  1532.0     0.000653    1288.75598       1553.11096
  1532.0     0.000653    1289.02563       1542.61475
  1528.0     0.000654    1289.27258       1532.03564
  1529.0     0.000654    1289.49695       1522.74036
  1545.0     0.000647    1289.69873       1514.82532
  1588.0     0.000630    1289.87817       1507.30762
  1668.0     0.000600    1290.03528       1499.04089
  1780.0     0.000562    1290.17004       1489.28284
  1901.0     0.000526    1290.28271       1478.44458
  1992.0     0.000502    1290.37317       1467.55029
  2017.0     0.000496    1290.44165       1457.93274
  1964.0     0.000509    1290.48816       1451.39099
  1858.0     0.000538    1290.51294       1449.85608
  1743.0     0.000574    1290.51611       1455.43152
  1651.0     0.000606    1290.49768       1469.72839
  1597.0     0.000626    1290.45789       1493.45325
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  1360.0     0.000735    1201.01123       1351.28333
  1372.0     0.000729    1201.06494       1363.49756
  1390.0     0.000719    1201.13196       1378.20178
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  1629.0     0.000614    1202.13306       1545.41858
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  1759.0     0.000569    1202.71399       1626.73193
  1888.0     0.000530    1202.93152       1687.01062
  2088.0     0.000479    1203.16077       1783.62952
  2375.0     0.000421    1203.40161       1931.53662
  2740.0     0.000365    1203.65393       2142.72925
  3137.0     0.0003188   1203.91748       2418.24683
  3478.0     0.0002875   1204.19214       2739.20630
  3650.0     0.0002740   1204.47766       3053.03345
  3585.0     0.0002789   1204.77405       3265.56201
  3295.0     0.0003035   1205.08118       3280.18481
  2873.0     0.0003481   1205.39868       3091.86621
  2441.0     0.000410    1205.72644       2795.46167
  2091.0     0.000478    1206.06433       2489.52710
  1859.0     0.000538    1206.41223       2229.97656
  1736.0     0.000576    1206.76990       2036.20935
  1689.0     0.000592    1207.13708       1905.13452
  1686.0     0.000593    1207.51379       1822.51990
  1700.0     0.000588    1207.89966       1772.71313
  1714.0     0.000583    1208.29456       1745.20227
  1720.0     0.000581    1208.69824       1733.62659
  1718.0     0.000582    1209.11072       1733.34888
  1717.0     0.000582    1209.53162       1741.93848
  1726.0     0.000579    1209.96082       1761.16394
  1756.0     0.000569    1210.39795       1794.94299
  1813.0     0.000552    1210.84302       1845.41919
  1895.0     0.000528    1211.29590       1907.57703
  1988.0     0.000503    1211.75610       1971.36377
  2076.0     0.000482    1212.22363       2018.44385
  2138.0     0.000468    1212.69836       2029.54492
  2161.0     0.000463    1213.17981       1999.76294
  2151.0     0.000465    1213.66785       1943.13770
  2123.0     0.000471    1214.16248       1880.81641
  2102.0     0.000476    1214.66333       1829.02722
  2110.0     0.000474    1215.17017       1797.21057
  2160.0     0.000463    1215.68286       1789.02722
  2242.0     0.000446    1216.20117       1803.22241
  2325.0     0.000430    1216.72485       1833.14368
  2370.0     0.000422    1217.25378       1865.76660
  2350.0     0.000426    1217.78772       1883.39893
  2265.0     0.000442    1218.32629       1873.63062
  2140.0     0.000467    1218.86963       1840.04956
  2009.0     0.000498    1219.41724       1798.09009
  1893.0     0.000528    1219.96887       1762.94592
  1807.0     0.000553    1220.52454       1744.11987
  1751.0     0.000571    1221.08398       1746.16431
  1731.0     0.000578    1221.64685       1769.67883
  1747.0     0.000572    1222.21301       1812.59045
  1796.0     0.000557    1222.78235       1869.34497
  1862.0     0.000537    1223.35449       1930.37427
  1931.0     0.000518    1223.92920       1982.52478
  1989.0     0.000503    1224.50659       2013.47705
  2027.0     0.000493    1225.08606       2019.03003
  2043.0     0.000489    1225.66772       2004.77271
  2035.0     0.000491    1226.25122       1978.84717
  2002.0     0.000500    1226.83630       1944.00464
  1949.0     0.000513    1227.42273       1898.83032
  1886.0     0.000530    1228.01062       1842.61365
  1823.0     0.000549    1228.59937       1780.16907
  1769.0     0.000565    1229.18896       1718.90308
  1729.0     0.000578    1229.77942       1664.17981
  1700.0     0.000588    1230.37012       1618.15906
  1680.0     0.000595    1230.96118       1580.13464
  1659.0     0.000603    1231.55225       1547.33826
  1625.0     0.000615    1232.14331       1516.90808
  1580.0     0.000633    1232.73389       1488.15503
  1527.0     0.000655    1233.32410       1462.09143
  1474.0     0.000678    1233.91370       1440.53870
  1427.0     0.000701    1234.50232       1423.75879
  1390.0     0.000719    1235.08984       1411.66809
  1363.0     0.000734    1235.67639       1403.81323
  1347.0     0.000742    1236.26147       1399.54541
  1341.0     0.000746    1236.84485       1398.00610
  1341.0     0.000746    1237.42664       1398.39954
  1346.0     0.000743    1238.00659       1399.81934
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  1341.0     0.000746    1240.30396       1408.23779
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  1342.0     0.000745    1243.66699       1492.65906
  1351.0     0.000740    1244.21606       1515.78687
  1357.0     0.000737    1244.76135       1538.01282
  1361.0     0.000735    1245.30286       1558.35632
  1365.0     0.000733    1245.84058       1576.65723
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  1479.0     0.000676    1248.46619       1631.76660
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  1883.0     0.000531    1250.97778       1736.33496
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  1941.0     0.000515    1252.42517       1837.77039
  1865.0     0.000536    1252.89734       1827.43945
  1768.0     0.000566    1253.36401       1789.63440
  1671.0     0.000598    1253.82544       1736.99487
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  1537.0     0.000651    1254.73181       1631.52881
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  1512.0     0.000661    1255.61597       1554.24951
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  1567.0     0.000638    1257.72729       1470.55115
  1536.0     0.000651    1258.13220       1466.36548
  1505.0     0.000664    1258.53137       1465.85278
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  1478.0     0.000677    1259.31213       1476.28955
  1487.0     0.000672    1259.69373       1486.76367
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  1652.0     0.000605    1261.51392       1587.43921
  1708.0     0.000585    1261.86047       1623.89978
  1770.0     0.000565    1262.20117       1669.01697
  1834.0     0.000545    1262.53613       1723.58252
  1897.0     0.000527    1262.86536       1787.86975
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  2028.0     0.000493    1263.50671       1938.80347
  2104.0     0.000475    1263.81885       2016.36414
  2189.0     0.000457    1264.12549       2084.62354
  2263.0     0.000442    1264.42651       2134.35962
  2299.0     0.000435    1264.72205       2158.47241
  2273.0     0.000440    1265.01208       2153.37256
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  1445.0     0.000692    1271.25098       1485.08691
  1459.0     0.000685    1271.42175       1478.97192
  1475.0     0.000678    1271.59009       1473.84460
  1484.0     0.000674    1271.75635       1468.60840
  1483.0     0.000674    1271.92065       1462.42834
  1473.0     0.000679    1272.08301       1455.02954
  1458.0     0.000686    1272.24365       1447.05078
  1440.0     0.000694    1272.40259       1439.01221
  1421.0     0.000704    1272.56018       1431.60657
  1404.0     0.000712    1272.71655       1425.52844
  1392.0     0.000718    1272.87170       1421.17188
  1381.0     0.000724    1273.02600       1418.63013
  1372.0     0.000729    1273.17944       1418.20117
  1365.0     0.000733    1273.33228       1419.40149
  1358.0     0.000736    1273.48462       1422.51147
  1351.0     0.000740    1273.63672       1427.58350
  1345.0     0.000743    1273.78857       1434.74121
  1343.0     0.000745    1273.94043       1443.90881
  1348.0     0.000742    1274.09253       1454.73230
  1361.0     0.000735    1274.24500       1466.17468
  1384.0     0.000723    1274.39795       1478.15112
  1416.0     0.000706    1274.55164       1489.44714
  1457.0     0.000686    1274.70618       1499.56543
  1498.0     0.000668    1274.86169       1508.43701
  1532.0     0.000653    1275.01843       1516.16528
  1550.0     0.000645    1275.17651       1522.64307
  1551.0     0.000645    1275.33618       1527.66284
  1539.0     0.000650    1275.49756       1530.49390
  1524.0     0.000656    1275.66077       1532.07178
  1518.0     0.000659    1275.82605       1533.54224
  1529.0     0.000654    1275.99353       1535.49622
  1557.0     0.000642    1276.16345       1537.89612
  1602.0     0.000624    1276.33582       1539.90735
  1652.0     0.000605    1276.51099       1540.52332
  1692.0     0.000591    1276.68909       1538.92029
  1709.0     0.000585    1276.87024       1534.90857
  1696.0     0.000590    1277.05457       1528.52783
  1660.0     0.000602    1277.24231       1520.56665
  1609.0     0.000622    1277.43372       1512.08826
  1559.0     0.000641    1277.62878       1504.34607
  1519.0     0.000658    1277.82776       1498.53674
  1496.0     0.000668    1278.03076       1495.84167
  1491.0     0.000671    1278.23792       1497.29626
  1504.0     0.000665    1278.44958       1504.14380
  1533.0     0.000652    1278.66577       1517.56079
  1576.0     0.000635    1278.88660       1539.07141
  1634.0     0.000612    1279.11230       1570.03345
  1701.0     0.000588    1279.34314       1611.19104
  1769.0     0.000565    1279.57898       1662.85156
  1833.0     0.000546    1279.82031       1724.55652
  1879.0     0.000532    1280.06689       1793.01489
  1897.0     0.000527    1280.31934       1860.64050
  1883.0     0.000531    1280.57739       1915.08728
  1835.0     0.000545    1280.84143       1940.73718
  1766.0     0.000566    1281.11145       1930.34741
  1691.0     0.000591    1281.38770       1891.16736
  1627.0     0.000615    1281.67029       1839.30640
  1588.0     0.000630    1281.95935       1789.34009
  1578.0     0.000634    1282.25513       1749.98645
  1595.0     0.000627    1282.55750       1724.87280
  1629.0     0.000614    1282.86682       1713.91650
  1671.0     0.000598    1283.18311       1714.57471
  1712.0     0.000584    1283.50659       1721.51794
  1747.0     0.000572    1283.83716       1726.94592
  1774.0     0.000564    1284.17529       1723.88574
  1792.0     0.000558    1284.52075       1709.81897
  1802.0     0.000555    1284.87390       1687.43738
  1796.0     0.000557    1285.23462       1659.87646
  1773.0     0.000564    1285.60327       1629.66711
  1733.0     0.000577    1285.97974       1599.24463
  1680.0     0.000595    1286.36438       1570.37830
  1626.0     0.000615    1286.75696       1544.88672
  1578.0     0.000634    1287.15784       1523.50708
  1538.0     0.000650    1287.56702       1506.11255
  1509.0     0.000663    1287.98462       1492.13171
  1486.0     0.000673    1288.41064       1481.32166
  1470.0     0.000680    1288.84521       1473.81897
  1460.0     0.000685    1289.28845       1470.18896
  1458.0     0.000686    1289.74036       1470.75659
  1466.0     0.000682    1290.20117       1475.67041
  1487.0     0.000672    1290.67078       1485.02185
  1521.0     0.000657    1291.14929       1498.89905
  1568.0     0.000638    1291.63672       1516.81238
  1620.0     0.000617    1292.13330       1537.21338
  1663.0     0.000601    1292.63892       1556.98364
  1685.0     0.000593    1293.15356       1571.97632
  1680.0     0.000595    1293.67761       1578.93396
  1649.0     0.000606    1294.21069       1577.81030
  1604.0     0.000623    1294.75317       1571.72937
  1557.0     0.000642    1295.30493       1564.79126
  1523.0     0.000657    1295.86597       1560.60999
  1504.0     0.000665    1296.43640       1561.46741
  1504.0     0.000665    1297.01624       1568.31506
  1521.0     0.000657    1297.60535       1580.70020
  1548.0     0.000646    1298.20398       1596.59705
  1574.0     0.000635    1298.81213       1612.46057
  1590.0     0.000629    1299.42957       1623.71997
  1590.0     0.000629    1300.05640       1627.63623
  1576.0     0.000635    1300.69275       1624.76807
  1554.0     0.000644    1301.33862       1618.25793
  1533.0     0.000652    1301.99365       1611.76819
  1523.0     0.000657    1302.65833       1607.83667
  1524.0     0.000656    1303.33228       1607.60864
  1530.0     0.000654    1304.01563       1608.84631
  1532.0     0.000653    1304.70825       1609.05200
  1526.0     0.000655    1305.41028       1605.02734
  1509.0     0.000663    1306.12158       1595.53674
  1486.0     0.000673    1306.84204       1581.51904
  1460.0     0.000685    1307.57178       1565.15381
  1436.0     0.000696    1308.31055       1548.50720
  1418.0     0.000705    1309.05847       1533.12622
  1407.0     0.000711    1309.81555       1519.98145
  1406.0     0.000711    1310.58142       1509.46021
  1414.0     0.000707    1311.35632       1501.48425
  1431.0     0.000699    1312.14014       1495.67493
  1452.0     0.000689    1312.93250       1491.58911
  1471.0     0.000680    1313.73364       1488.88977
  1484.0     0.000674    1314.54358       1487.35693
  1489.0     0.000672    1315.36194       1486.83044
  1488.0     0.000672    1316.18872       1487.16211
  1485.0     0.000673    1317.02405       1488.47400
  1485.0     0.000673    1317.86743       1490.91980
  1493.0     0.000670    1318.71899       1494.51794
  1511.0     0.000662    1319.57874       1500.49597
  1537.0     0.000651    1320.44641       1508.12329
  1569.0     0.000637    1321.32190       1516.80530
  1600.0     0.000625    1322.20520       1525.95837
  1625.0     0.000615    1323.09595       1535.71411
  1642.0     0.000609    1323.99426       1546.98889
  1654.0     0.000605    1324.90002       1560.49817
  1663.0     0.000601    1325.81299       1577.16333
  1677.0     0.000596    1326.73303       1597.66724
  1703.0     0.000587    1327.66003       1622.73804
  1744.0     0.000573    1328.59399       1652.13464
  1800.0     0.000556    1329.53442       1684.11340
  1863.0     0.000537    1330.48157       1715.06042
  1917.0     0.000522    1331.43506       1740.11414
  1944.0     0.000514    1332.39478       1755.19788
  1936.0     0.000517    1333.36047       1759.24915
  1893.0     0.000528    1334.33228       1754.22900
  1825.0     0.000548    1335.30969       1742.99353
  1747.0     0.000572    1336.29272       1727.71619
  1672.0     0.000598    1337.28137       1710.05615
  1609.0     0.000622    1338.27502       1690.95789
  1561.0     0.000641    1339.27380       1671.48633
  1526.0     0.000655    1340.27759       1653.16150
  1501.0     0.000666    1341.28601       1636.70264
  1485.0     0.000673    1342.29895       1623.13269
  1477.0     0.000677    1343.31641       1613.30444
  1475.0     0.000678    1344.33777       1607.30188
  1478.0     0.000677    1345.36316       1604.80151
  1485.0     0.000673    1346.39246       1605.47375
  1494.0     0.000669    1347.42529       1606.90210
  1505.0     0.000664    1348.46143       1608.11658
  1519.0     0.000658    1349.50073       1607.71753
  1533.0     0.000652    1350.54309       1604.51929
  1542.0     0.000649    1351.58813       1598.09875
  1543.0     0.000648    1352.63574       1589.07898
  1534.0     0.000652    1353.68591       1578.14868
  1518.0     0.000659    1354.73804       1566.52734
  1500.0     0.000667    1355.79211       1554.70374
  1484.0     0.000674    1356.84790       1543.99304
  1475.0     0.000678    1357.90527       1534.57312
  1479.0     0.000676    1358.96375       1527.28955
  1496.0     0.000668    1360.02356       1520.75354
  1529.0     0.000654    1361.08398       1515.41064
  1575.0     0.000635    1362.14514       1510.27930
  1628.0     0.000614    1363.20679       1507.26465
  1683.0     0.000594    1364.26843       1505.52136
  1732.0     0.000577    1365.33008       1505.48962
  1764.0     0.000567    1366.39148       1507.64294
  1773.0     0.000564    1367.45239       1512.21545
  1762.0     0.000568    1368.51245       1519.73438
  1735.0     0.000576    1369.57178       1530.52625
  1702.0     0.000588    1370.62976       1544.79089
  1678.0     0.000596    1371.68640       1562.35181
  1672.0     0.000598    1372.74146       1582.72278
  1690.0     0.000592    1373.79443       1605.43799
  1726.0     0.000579    1374.84546       1628.62952
  1768.0     0.000566    1375.89404       1649.84570
  1798.0     0.000556    1376.94019       1666.36560
  1805.0     0.000554    1377.98340       1675.78589
  1787.0     0.000560    1379.02368       1678.36450
  1756.0     0.000569    1380.06067       1676.07678
  1726.0     0.000579    1381.09424       1671.18420
  1710.0     0.000585    1382.12390       1664.86230
  1708.0     0.000585    1383.14990       1657.10303
  1713.0     0.000584    1384.17151       1647.59033
  1716.0     0.000583    1385.18872       1636.53796
  1710.0     0.000585    1386.20142       1624.82153
  1690.0     0.000592    1387.20911       1613.52930
  1658.0     0.000603    1388.21179       1603.66772
  1620.0     0.000617    1389.20923       1595.69763
  1583.0     0.000632    1390.20105       1589.78931
  1552.0     0.000644    1391.18713       1585.80505
  1532.0     0.000653    1392.16736       1583.07056
  1522.0     0.000657    1393.14124       1580.90491
  1518.0     0.000659    1394.10864       1578.42639
  1518.0     0.000659    1395.06970       1575.45325
  1518.0     0.000659    1396.02368       1572.27991
  1521.0     0.000657    1396.97058       1569.78271
  1528.0     0.000654    1397.91040       1568.25330
  1538.0     0.000650    1398.84253       1567.97498
  1549.0     0.000646    1399.76697       1568.28357
  1557.0     0.000642    1400.68359       1568.03552
  1557.0     0.000642    1401.59229       1565.76624
  1547.0     0.000646    1402.49243       1561.47266
  1532.0     0.000653    1403.38416       1556.39404
  1515.0     0.000660    1404.26733       1551.79370
  1501.0     0.000666    1405.14148       1548.77490
  1490.0     0.000671    1406.00647       1547.99878
  1485.0     0.000673    1406.86243       1549.85229
  1490.0     0.000671    1407.70874       1554.47510
  1502.0     0.000666    1408.54541       1561.83057
  1522.0     0.000657    1409.37244       1572.05457
  1544.0     0.000648    1410.18933       1584.84692
  1567.0     0.000638    1410.99597       1600.01147
  1591.0     0.000629    1411.79248       1617.29248
  1617.0     0.000618    1412.57825       1636.39380
  1646.0     0.000608    1413.35352       1656.96143
  1682.0     0.000595    1414.11792       1679.55078
  1723.0     0.000580    1414.87122       1704.54297
  1772.0     0.000564    1415.61340       1732.42603
  1827.0     0.000547    1416.34448       1763.62671
  1881.0     0.000532    1417.06384       1797.65662
  1922.0     0.000520    1417.77173       1832.59998
  1937.0     0.000516    1418.46802       1862.88330
  1926.0     0.000519    1419.15222       1882.16199
  1892.0     0.000529    1419.82446       1886.07605
  1850.0     0.000541    1420.48462       1876.95569
  1812.0     0.000552    1421.13245       1861.27393
  1788.0     0.000559    1421.76794       1844.29822
  1781.0     0.000561    1422.39099       1827.79968
  1784.0     0.000561    1423.00146       1810.76025
  1791.0     0.000558    1423.59900       1791.34619
  1793.0     0.000558    1424.18384       1771.08423
  1786.0     0.000560    1424.75586       1752.90027
  1772.0     0.000564    1425.31470       1739.73120
  1757.0     0.000569    1425.86047       1733.14148
  1749.0     0.000572    1426.39319       1734.01221
  1753.0     0.000570    1426.91235       1741.37329
  1774.0     0.000564    1427.41833       1754.32642
  1808.0     0.000553    1427.91089       1770.64600
  1846.0     0.000542    1428.38989       1788.74280
  1882.0     0.000531    1428.85522       1808.84314
  1908.0     0.000524    1429.30713       1833.28259
  1926.0     0.000519    1429.74512       1864.97314
  1939.0     0.000516    1430.16956       1905.74048
  1950.0     0.000513    1430.58008       1955.35547
  1960.0     0.000510    1430.97693       2010.73987
  1972.0     0.000507    1431.35974       2065.18530
  1984.0     0.000504    1431.72876       2108.74634
  1995.0     0.000501    1432.08386       2132.76660
  2001.0     0.000500    1432.42493       2134.10034
  1998.0     0.000501    1432.75208       2115.86914
  1980.0     0.000505    1433.06519       2084.15601
  1946.0     0.000514    1433.36438       2045.63049
  1901.0     0.000526    1433.64954       2005.93701
  1854.0     0.000539    1433.92078       1969.57422
  1814.0     0.000551    1434.17798       1939.22375
  1785.0     0.000560    1434.42114       1914.91663
  1769.0     0.000565    1434.65051       1896.87952
  1762.0     0.000568    1434.86584       1884.35876
  1759.0     0.000569    1435.06726       1876.83960
  1757.0     0.000569    1435.25476       1873.33972
  1756.0     0.000569    1435.42847       1872.31750
  1758.0     0.000569    1435.58826       1872.59326
  1767.0     0.000566    1435.73438       1874.06860
  1790.0     0.000559    1435.86670       1876.76160
  1833.0     0.000546    1435.98547       1879.85461
  1901.0     0.000526    1436.09058       1881.38635
  1985.0     0.000504    1436.18213       1879.09424
  2068.0     0.000484    1436.26025       1871.87756
  2126.0     0.000470    1436.32495       1859.91992
  2140.0     0.000467    1436.37622       1845.36682
  2107.0     0.000475    1436.41431       1830.28113
  2040.0     0.000490    1436.43933       1816.77930
  1962.0     0.000510    1436.45117       1806.31433
  1898.0     0.000527    1436.45020       1799.56982
  1862.0     0.000537    1436.43616       1796.04883
  1850.0     0.000541    1436.40942       1794.72314
  1849.0     0.000541    1436.37012       1794.16394
  1850.0     0.000541    1436.31812       1794.05591
  1846.0     0.000542    1436.25378       1795.46777
  1836.0     0.000545    1436.17712       1800.72498
  1823.0     0.000549    1436.08838       1811.93542
  1812.0     0.000552    1435.98743       1830.20532
  1810.0     0.000552    1435.87463       1855.22156
  1816.0     0.000551    1435.75012       1885.33191
  1837.0     0.000544    1435.61389       1918.02759
  1877.0     0.000533    1435.46619       1951.54468
  1938.0     0.000516    1435.30713       1984.89734
  2018.0     0.000496    1435.13696       2015.96863
  2101.0     0.000476    1434.95569       2039.98804
  2164.0     0.000462    1434.76355       2051.03418
  2185.0     0.000458    1434.56079       2044.84644
  2157.0     0.000464    1434.34741       2021.78271
  2090.0     0.000478    1434.12366       1986.92786
  2008.0     0.000498    1433.88977       1946.67651
  1932.0     0.000518    1433.64587       1906.62964
  1876.0     0.000533    1433.39221       1869.31750
  1835.0     0.000545    1433.12891       1836.25269
  1803.0     0.000555    1432.85608       1807.75879
  1775.0     0.000563    1432.57397       1783.46216
  1748.0     0.000572    1432.28296       1763.10229
  1727.0     0.000579    1431.98291       1745.32324
  1717.0     0.000582    1431.67432       1729.79541
  1725.0     0.000580    1431.35730       1716.17932
  1742.0     0.000574    1431.03186       1704.34058
  1760.0     0.000568    1430.69849       1694.37756
  1768.0     0.000566    1430.35730       1686.42114
  1762.0     0.000568    1430.00842       1680.09436
  1744.0     0.000573    1429.65222       1675.65881
  1722.0     0.000581    1429.28882       1673.30579
  1705.0     0.000587    1428.91833       1673.02100
  1697.0     0.000589    1428.54126       1674.66699
  1695.0     0.000590    1428.15759       1676.88782
  1696.0     0.000590    1427.76758       1677.73779
  1695.0     0.000590    1427.37158       1675.98718
  1689.0     0.000592    1426.96973       1672.08374
  1679.0     0.000596    1426.56226       1667.99585
  1666.0     0.000600    1426.14941       1665.32312
  1653.0     0.000605    1425.73145       1665.14124
  1642.0     0.000609    1425.30859       1668.33716
  1630.0     0.000613    1424.88098       1675.18994
  1621.0     0.000617    1424.44897       1686.45483
  1617.0     0.000618    1424.01282       1702.48950
  1622.0     0.000617    1423.57263       1723.38440
  1638.0     0.000611    1423.12878       1748.57825
  1663.0     0.000601    1422.68152       1776.80688
  1694.0     0.000590    1422.23096       1806.26257
  1725.0     0.000580    1421.77734       1834.27136
  1750.0     0.000571    1421.32104       1859.14917
  1767.0     0.000566    1420.86218       1878.41455
  1784.0     0.000561    1420.40112       1890.70471
  1805.0     0.000554    1419.93799       1894.79468
  1832.0     0.000546    1419.47302       1890.23523
  1859.0     0.000538    1419.00647       1877.82751
  1881.0     0.000532    1418.53870       1859.84900
  1891.0     0.000529    1418.06982       1839.26868
  1889.0     0.000529    1417.60022       1818.84229
  1879.0     0.000532    1417.13000       1800.63171
  1868.0     0.000535    1416.65930       1785.57336
  1867.0     0.000536    1416.18860       1773.91187
  1877.0     0.000533    1415.71802       1765.21179
  1900.0     0.000526    1415.24780       1758.52332
  1924.0     0.000520    1414.77808       1752.72400
  1930.0     0.000518    1414.30933       1746.89502
  1911.0     0.000523    1413.84155       1740.68066
  1868.0     0.000535    1413.37500       1734.36414
  1807.0     0.000553    1412.91016       1728.40479
  1744.0     0.000573    1412.44690       1723.29578
  1689.0     0.000592    1411.98560       1719.15588
  1650.0     0.000606    1411.52661       1715.83032
  1625.0     0.000615    1411.06995       1713.04114
  1610.0     0.000621    1410.61584       1710.50024
  1602.0     0.000624    1410.16467       1707.88245
  1596.0     0.000627    1409.71655       1704.86182
  1588.0     0.000630    1409.27173       1700.61804
  1575.0     0.000635    1408.83032       1695.13098
  1561.0     0.000641    1408.39270       1689.11768
  1544.0     0.000648    1407.95874       1683.38049
  1529.0     0.000654    1407.52905       1678.70288
  1519.0     0.000658    1407.10364       1675.68689
  1513.0     0.000661    1406.68274       1674.70776
  1514.0     0.000661    1406.26636       1676.46558
  1519.0     0.000658    1405.85498       1682.11523
  1530.0     0.000654    1405.44861       1692.11926
  1547.0     0.000646    1405.04749       1706.86938
  1572.0     0.000636    1404.65173       1726.15125
  1606.0     0.000623    1404.26147       1749.10132
  1646.0     0.000608    1403.87708       1774.32019
  1689.0     0.000592    1403.49854       1799.66382
  1733.0     0.000577    1403.12598       1822.18152
  1769.0     0.000565    1402.75977       1837.83752
  1794.0     0.000557    1402.40002       1843.25244
  1802.0     0.000555    1402.04663       1837.86292
  1796.0     0.000557    1401.70007       1824.10083
  1781.0     0.000561    1401.36035       1805.21826
  1766.0     0.000566    1401.02747       1783.85938
  1753.0     0.000570    1400.70178       1761.30859
  1742.0     0.000574    1400.38330       1738.23242
  1730.0     0.000578    1400.07214       1715.69373
  1714.0     0.000583    1399.76843       1694.66870
  1694.0     0.000590    1399.47229       1674.33911
  1671.0     0.000598    1399.18396       1656.28516
  1654.0     0.000605    1398.90332       1640.99402
  1647.0     0.000607    1398.63074       1628.73193
  1658.0     0.000603    1398.36597       1619.56958
  1691.0     0.000591    1398.10938       1613.43640
  1742.0     0.000574    1397.86096       1610.33374
  1803.0     0.000555    1397.62073       1610.59241
  1865.0     0.000536    1397.38892       1614.50952
  1917.0     0.000522    1397.16553       1622.46594
  1946.0     0.000514    1396.95056       1634.67578
  1950.0     0.000513    1396.74402       1650.73950
  1930.0     0.000518    1396.54626       1670.10876
  1896.0     0.000527    1396.35693       1691.79260
  1861.0     0.000537    1396.17639       1714.86145
  1833.0     0.000546    1396.00452       1738.68921
  1819.0     0.000550    1395.84143       1762.80688
  1817.0     0.000550    1395.68713       1786.42004
  1824.0     0.000548    1395.54150       1808.20654
  1832.0     0.000546    1395.40479       1826.92395
  1836.0     0.000545    1395.27686       1841.16711
  1834.0     0.000545    1395.15771       1850.69763
  1829.0     0.000547    1395.04749       1855.14807
  1828.0     0.000547    1394.94604       1854.13892
  1826.0     0.000548    1394.85339       1847.22656
  1821.0     0.000549    1394.76953       1834.59985
  1806.0     0.000554    1394.69446       1817.01611
  1780.0     0.000562    1394.62805       1795.97070
  1743.0     0.000574    1394.57043       1773.35730
  1700.0     0.000588    1394.52148       1751.06470
  1660.0     0.000602    1394.48108       1730.52795
  1630.0     0.000613    1394.44934       1712.79578
  1615.0     0.000619    1394.42603       1698.49561
  1610.0     0.000621    1394.41113       1688.00964
  1613.0     0.000620    1394.40466       1681.59387
  1621.0     0.000617    1394.40662       1679.42822
  1633.0     0.000612    1394.41663       1681.65552
  1651.0     0.000606    1394.43494       1688.21887
  1676.0     0.000597    1394.46118       1698.98096
  1707.0     0.000586    1394.49536       1713.52307
  1741.0     0.000574    1394.53748       1731.15930
  1776.0     0.000563    1394.58728       1751.18030
  1807.0     0.000553    1394.64478       1772.56787
  1832.0     0.000546    1394.70984       1795.01013
  1852.0     0.000540    1394.78223       1818.58582
  1867.0     0.000536    1394.86194       1843.87427
  1885.0     0.000531    1394.94873       1871.25342
  1909.0     0.000524    1395.04260       1899.75439
  1939.0     0.000516    1395.14319       1926.66553
  1972.0     0.000507    1395.25061       1948.10583
  1998.0     0.000501    1395.36462       1960.19641
  2003.0     0.000499    1395.48486       1961.74097
  1980.0     0.000505    1395.61145       1953.76013
  1926.0     0.000519    1395.74414       1938.75085
  1855.0     0.000539    1395.88269       1919.46948
  1781.0     0.000561    1396.02698       1898.12134
  1721.0     0.000581    1396.17676       1876.21130
  1685.0     0.000593    1396.33179       1854.48901
  1673.0     0.000598    1396.49219       1834.05518
  1674.0     0.000597    1396.65735       1815.33850
  1676.0     0.000597    1396.82739       1798.94824
  1674.0     0.000597    1397.00195       1785.42346
  1668.0     0.000600    1397.18079       1775.13855
  1660.0     0.000602    1397.36389       1768.22717
  1656.0     0.000604    1397.55090       1764.55164
  1665.0     0.000601    1397.74146       1763.91260
  1687.0     0.000593    1397.93567       1766.33899
  1721.0     0.000581    1398.13306       1772.62085
  1762.0     0.000568    1398.33337       1783.99609
  1805.0     0.000554    1398.53650       1801.65063
  1850.0     0.000541    1398.74219       1826.11096
  1902.0     0.000526    1398.95020       1856.74976
  1963.0     0.000509    1399.16016       1891.11621
  2028.0     0.000493    1399.37207       1924.37183
  2092.0     0.000478    1399.58545       1949.37854
  2146.0     0.000466    1399.80017       1959.34766
  2183.0     0.000458    1400.01587       1952.02966
  2194.0     0.000456    1400.23230       1930.98779
  2180.0     0.000459    1400.44934       1902.71460
  2145.0     0.000466    1400.66650       1872.22253
  2092.0     0.000478    1400.88379       1842.84558
  2028.0     0.000493    1401.10071       1816.96069
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  1902.0     0.000526    1401.53259       1783.02527
  1864.0     0.000536    1401.74707       1777.22803
  1849.0     0.000541    1401.96008       1779.28577
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  1921.0     0.000521    1402.58789       1827.87207
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  2013.0     0.000497    1402.99438       1878.62097
  2053.0     0.000487    1403.19312       1898.65540
  2079.0     0.000481    1403.38855       1910.65601
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  2058.0     0.000486    1403.76794       1908.01868
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  1909.0     0.000524    1404.30457       1849.95313
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  1749.0     0.000572    1405.71729       1675.90234
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   0.0      .            .                .
   0.0      .            .                .
   0.0      .            .                .
   0.0      .            .                .
   0.0      .            .                .
   0.0      .            .                .
   0.0      .            .                .
_pd_meas_number_of_points              3274
_pd_proc_number_of_points              3274

_reflns_number_total                   1113
_reflns_limit_h_min                    0
_reflns_limit_h_max                    14
_reflns_limit_k_min                    0
_reflns_limit_k_max                    10
_reflns_limit_l_min                    0
_reflns_limit_l_max                    18
_reflns_d_resolution_high              0.995
_reflns_d_resolution_low               11.176
#--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--eof--#
